The invention relates to the field of
fiber material performance testing, in particular to a preparation method of an intermittently-graphitized
pitch-based carbon
fiber heat conduction sample and the sample, and the preparation method comprises the following steps: S1, winding
raw material fibers according to the composition of
pitch-based
carbon fibers to be tested; s2,
cutting and bundling are conducted respectively,
graphite paper is used for wrapping, and then PAN-based
carbon fibers are used for bundling; s3, carrying out intermittent graphitization treatment, folding and
cutting off, and then trimming; s5, a
polyimide adhesive tape is adopted for longitudinal spiral winding, tightening and wrapping to form a cylinder, and then
cutting is conducted; and S6,
polishing to obtain the
asphalt-based
graphite fiber heat conduction sample. The
asphalt-based carbon fiber is subjected to sample treatment before intermittent graphitization, the sample treatment comprises the processes of unwinding, winding, cutting and the like, and the corresponding processes of
fiber bundle binding, cutting and the like are performed after graphitization treatment to prepare the fiber heat conduction sample, so that the
asphalt-based carbon fiber is kept in a smooth state after graphitization treatment; meanwhile, the preparation efficiency of the fiber heat conduction sample is improved.