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High-performance silicon carbide composite kiln furniture material and preparation method thereof

A high-performance silicon carbide and kiln furniture technology, applied in the field of refractory materials, can solve the problems of high equipment requirements, low production costs, and high production costs, and achieve the effects of increased service life, strong oxidation resistance, and regular appearance

Inactive Publication Date: 2013-07-31
福州远程特耐砂轮有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to provide a high-performance silicon carbide composite kiln furniture and its preparation method, to solve the complex production technology of silicon nitride combined with silicon carbide and recrystallized silicon carbide products in the prior art, high equipment requirements, large investment, and production problems. Expensive, limited in the market promotion process, etc., the preparation method of the raw material formula of the present invention is scientific and reasonable, and the obtained high-performance silicon carbide composite kiln furniture material has high temperature resistance, small deformation, high strength, strong oxidation resistance, and regular shape , The service life is significantly improved; the preparation method of the new silicon carbide composite kiln furniture has better control of production technology, lower production cost, and good performance. It is believed that it has a good market prospect in the high-temperature kiln industry.

Method used

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Experimental program
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Effect test

preparation example Construction

[0012] The preparation method comprises the following steps:

[0013] (1) Mixing: put all the raw materials into the mixing machine according to the ratio of raw materials and mix them evenly;

[0014] (2) Trapped material: put the uniformly mixed material in step (1) in a closed state for 12-36 hours;

[0015] (3) Molding: put the materials that have been left still in step (2) into corresponding molds after weighing according to the materials required by different kiln furniture; during molding, the mold is vibrated and pressurized on both sides, and the extreme vibration force is 200-350KN, vibration time 1-30 seconds;

[0016] (4) Drying: drying the blank formed in step (3) at 80-120°C until the water content is less than 1%;

[0017] (5) Firing: sintering and forming at 1300-1650° C. to obtain the complex-phase high-temperature-resistant kiln furniture.

[0018] (6) Detection: The composite kiln furniture fired in the step (5) is tested according to the technical requi...

Embodiment 1

[0021] The production process of kiln furniture is:

[0022] (1) Mixing: Put the raw materials into the mixer according to the above ratio and mix them evenly; if 1000Kg of materials are configured, the weight of each material is as follows:

[0023] SiC 900Kg, Si 2 ON 2 and Al 2 TiO 5 Mix according to the ratio of 1:1 to reach a total amount of 98Kg, and the room temperature binder is 2Kg. Among the above 900Kg SiC, 500Kg of SiC particles with a particle size of 20 mesh, 400Kg of SiC fine powder with a particle size of 200 mesh, and the above 98Kg of SiC 2 ON 2 and Al 2 TiO 5 It is a fine powder of 7 μm, and the above-mentioned binder at room temperature is dextrin.

[0024] (2) Trapped material: the above-mentioned uniformly mixed material was left to stand in a closed state for 24 hours;

[0025] (3) Molding: The prepared materials are weighed according to the materials required by different kiln furniture and put into the corresponding molds for molding; during mo...

Embodiment 2

[0032] The production process of kiln furniture is:

[0033] (1) Mixing: Put the raw materials into the mixer according to the above ratio and mix them evenly; if 1000Kg of materials are configured, the weight of each material is as follows:

[0034] SiC 850Kg, Si 3 N 4 and Al 2 TiO 5 Mix according to the ratio of 1:1 to reach a total amount of 148Kg, and the normal temperature binder is 2Kg. Among the above-mentioned 850Kg SiC, 500Kg of SiC particles with a particle size of 20 mesh, 350Kg of SiC fine powder with a particle size of 200 mesh, and the above-mentioned 148Kg of SiC 3 N 4 and Al 2 TiO 5 7μm fine powder. The above-mentioned binder at room temperature is a polyvinyl alcohol PVA solution with a concentration of 10%.

[0035] (2) Trapped material: the above-mentioned uniformly mixed material was left to stand in a closed state for 24 hours;

[0036](3) Molding: The prepared materials are weighed according to the materials required by different kiln furniture ...

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PUM

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Abstract

The invention provides a high-performance silicon carbide composite kiln furniture material and a preparation method thereof, belonging to the technical field of refractory material. In the invention, silicon carbide and additives are taken as the main raw materials; a series of processes including mixing, ageing mixture, drying, and molding, sintering and testing are carried out to prepare high-performance silicon carbide composite kiln furniture. The kiln furniture refractory material in the invention has the performances of high-temperature resistance, small deformation, oxidation resistance, low hot expansion coefficient, high strength, high thermal shock stability and the like.

Description

technical field [0001] The invention relates to a high-performance silicon carbide composite kiln furniture material and a preparation method thereof, belonging to the technical field of refractory materials. Background technique [0002] The production of kiln furniture in my country's ceramic industry has a long history. It is used to support and protect refractory products in the firing process of ceramic products. Its performance and quality are directly related to the ceramic products to be fired. And it also has a great influence on the firing cost, so the quality of kiln furniture is very important. [0003] Kiln furniture is a special-shaped refractory material used to support and protect products in the firing process, which has an extremely important impact on product quality and energy consumption. Correspondingly, the existing kiln furniture is poor in thermal shock stability, unstable in size, short in service life, and poor in use effect. Generally, after 2030 ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B35/66C04B35/622C04B35/565
Inventor 黄朝晖郑宝乡刘艳改房明浩郑春和
Owner 福州远程特耐砂轮有限公司