Bicomponent addition type room curing silicon rubber and preparation method thereof
A room temperature curing, two-component technology, applied in the field of two-component addition type room temperature curing silicone rubber and its preparation, can solve the problems of lower production efficiency, environmental pollution, poor adhesion of addition type liquid silicone rubber, etc., and achieve good flow performance, high thermal conductivity
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Embodiment 1
[0023] Add 32.9 parts of allyl silicone oil, 30 parts of 400-mesh quartz powder, 35 parts of 800-mesh alumina in the stirred tank, stir and heat up to 100°C for half an hour; add 1.5 parts of pink and 0.6 parts of platinum catalyst after cooling down, and stir for 10 Discharge in minutes to obtain component A;
[0024] Add 33.9 parts of allyl silicone oil, 30 parts of 400-mesh quartz powder, 30 parts of 800-mesh alumina powder into the stirred tank, stir and raise the temperature to 100°C for half an hour, after cooling down, add 0.7 parts of vinyl ring, 1.8 parts of hydrogen-containing silicone oil, 3.2 parts of tackifier, 0.4 parts of anti-sedimentation agent, stirred for 10 minutes and discharged to obtain component B;
[0025] Mix the above A and B evenly according to the weight ratio of 1:1 to obtain the above-mentioned novel two-component addition room temperature curing silicone rubber.
Embodiment 2
[0027] Add 43 parts of allyl silicone oil, 30 parts of 600-mesh quartz powder, 25.1 parts of 800-mesh alumina into the stirred tank, stir and heat up to 100°C for half an hour; add 1.1 parts of iron black and 0.8 parts of platinum catalyst after cooling down, and stir After 10 minutes of discharge, component A is obtained;
[0028] Add 43 parts of allyl silicone oil, 25 parts of 600-mesh quartz powder, and 25 parts of 800-mesh alumina powder into the stirred tank, stir and heat up to 100°C for half an hour. After cooling down, add 0.5 parts of acetylene alcohol, 2.5 parts of hydrogen-containing Silicone oil, 3.5 parts of viscosifier, 0.5 parts of anti-sedimentation agent, stirred for 10 minutes and discharged to obtain component B;
[0029] Mix the above A and B evenly according to the weight ratio of 1:1 to obtain the above-mentioned novel two-component addition room temperature curing silicone rubber.
Embodiment 3
[0031] Add 54 parts of allyl silicone oil, 20 parts of 800-mesh quartz powder, and 23 parts of 800-mesh alumina into the stirred tank, stir and heat up to 100°C for half an hour; add 2 parts of carbon black and 1 part of platinum catalyst after cooling down, and stir After 10 minutes of discharge, component A is obtained;
[0032] Add 54 parts of allyl silicone oil, 20 parts of 800-mesh quartz powder, and 18 parts of 800-mesh alumina powder into the stirred tank, stir and raise the temperature to 100°C for half an hour. After cooling down, add 1 part of vinyl ring, 3 parts of hydrogen-containing silicone oil, 3.2 parts of tackifier, 0.8 parts of anti-sedimentation agent, stirred for 10 minutes and discharged to obtain component B;
[0033] Mix the above A and B evenly according to the weight ratio of 1:1 to obtain the above-mentioned novel two-component addition room temperature curing silicone rubber.
[0034] The technical parameters of the prepared silicone rubber are as f...
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