Novel technology for continuously producing nano powder by using ultra-high temperature plasma and preparation process thereof

A plasma and nano-powder technology, applied in the direction of plasma, chemical/physical/physical-chemical process of applying energy, electrical components, etc., can solve the problems of low utilization rate of plasma energy, low energy utilization, complex equipment, etc. Achieve the effect of reducing the amount of nano-metal powder, avoiding energy waste, and simple equipment structure

Inactive Publication Date: 2010-12-29
李立明
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, this equipment has the disadvantages of low utilization rate of plasma energy, large air volume gas charging system and medium frequency induction heating system cannot exert the due 100% efficiency
The plasma system of CN100457339C patent only utilizes the medium-frequency induction heating system in the high-temperature plasma evaporation patented equipment to exist in the metal liquid in the water-cooled crucible after being liquefied at a high temperature by the medium-frequency heating system. Heat conduction and a large amount of heat conduction of the water-cooled crucible lead to a low utilization rate of high-temperature heat of the plasma, and only a small amount of metal vapor can be formed. The gas filling system of the CN100457339C equipment is used to continuously produce nano-metal powders with a very low output, so that the patented equipment The large air volume inflation system cannot exert 100% efficiency, CN100457339C patent equipment has repeated heating, low energy utilization, low yield, high production cost, and complicated equipment
[0005] Based on the above analysis, it can be found that the current domestic production and research equipment patents have not completely solved the problems of high quality, high yield, high cost, etc.

Method used

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  • Novel technology for continuously producing nano powder by using ultra-high temperature plasma and preparation process thereof
  • Novel technology for continuously producing nano powder by using ultra-high temperature plasma and preparation process thereof

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Embodiment Construction

[0036] Working process of the present invention is:

[0037] 1. Seal and evacuate the vacuum powder making chamber, and the vacuum measurement system stops after reaching the set vacuum degree (2.5*10-4Pa);

[0038] 2. Fill in the specific gas (Ar.N2.He.H2.NH3.CH4) for the production of nano-metal powder and stop when the set pressure is reached;

[0039] 3. Turn on the cooling water circulation system; 4. Turn on the nano metal powder cleaning system; 5. Turn on the nano metal powder collection system;

[0040] 6. Turn on the plasma power supply system; 7. Turn on the plasma gun system; 8. Turn on the plasma gun feeding system;

[0041] The ultra-high temperature compression arc (16000-32000K) generated by the plasma gun directly vaporizes the metal powder passing through the plasma gun to generate high-temperature metal vapor. Collision with large air volume gas molecules and the inner wall of the water cooling cycle loses energy, forms clusters, condenses into nano metal po...

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Abstract

The invention discloses novel technology for continuously producing nano powder by using ultra-high temperature plasma and a preparation process thereof. The technology is implemented by a device consisting of an electrical control system, a vacuum pumping and measuring system, an gas charging system, an ultra-high temperature plasma heating, evaporating and pulverizing system, a high air-flow cooling and circulating system, a water cooling and circulating system, a nano powder supplementing and collecting system, a powder cleaning system and a vacuum packaging and storing system. High vacuum is adopted in the embodiment of the invention and the method comprises the following steps of: directly heating metal powder by using the ultra-high temperature plasma to form metal vapor quickly; and colliding the metal vapor quickly with high air-flow gas molecules to make the metal vapor loose energy and form clusters by using the high air-flow cooling and circulating system and water cooling circulation, and condensing the clusters into the nano metal powder. Metal hydride nano powder, metal nitride nano powder, metal oxide nano powder and pure metal nano powder can be produced by using different protective gases. Compared with the prior art, the nano metal powder produced by the method has the advantages of difficult agglomeration, simple process, high purity, convenient operation and maintenance, low production cost, easy realization of large-scale industrial production and wide popularization.

Description

technical field [0001] The present invention relates to a new technology for continuous production of nano-powder by using ultra-high temperature plasma and its preparation process for continuous production: nano-pure metal powder, nano-metal hydride powder, nano-metal nitride powder, and nano-metal oxide powder The preparation technology is specifically a process and equipment for the industrial production of nanometer metal powder. Background technique [0002] Nanopowder refers to ultrafine particles with an average particle size below 100nm. Due to its small size, small number of atoms in the particle, and many atoms distributed on the surface, its surface area effect, volume effect and small size effect make it have different properties from conventional bulk and micropowder materials. It has many new and extremely important application values ​​in the fields of aviation, aerospace, military industry, materials, metallurgy, chemical industry, medicine, etc., and is kno...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/14H05H1/00B01J19/08
Inventor 李立明
Owner 李立明
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