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Directional solidifying crystallization method of metal alloy magnet and device for implementing same

A technology for directional solidification of metal alloys, applied in the field of directional solidification and crystallization of metal alloy magnets and devices implementing the method, which can solve the problems of uneven cooling, large temperature difference between the surface and core of metal alloy magnets, and the degree of crystal orientation needs to be improved. problem, to achieve the effect of overcoming the temperature gradient is too small

Inactive Publication Date: 2011-02-09
NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The grain size obtained by this method is smaller, the grain boundary is straighter than the previous two methods, and the columnar grain size is longer than them, but there is a problem of large temperature difference between the surface and the core of the metal alloy magnet and uneven cooling.
[0007] In addition, there are problems such as the specific gravity segregation of the metal alloy liquid in the above method, and the degree of crystal orientation of the metal alloy in the directional solidification and crystallization process needs to be improved.

Method used

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  • Directional solidifying crystallization method of metal alloy magnet and device for implementing same
  • Directional solidifying crystallization method of metal alloy magnet and device for implementing same
  • Directional solidifying crystallization method of metal alloy magnet and device for implementing same

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Embodiment 1

[0034] use Figure 1 to Figure 3 The device for implementing the method of directional solidification and crystallization of metal alloy magnets as shown, performs directional solidification and crystallization of a rod-shaped alnico magnet with a diameter of 10 mm and a length of 300 mm, wherein the current of the high-frequency induction power supply is 60A, and the lifting equipment is The speed of 2 mm / min moves downward, the cooling body is liquid cooling water, the distance from the induction coil to the cooling water surface is 60 mm, the magnetic induction of the transverse magnet on the periphery of the induction coil 6 is 2T, and the longitudinal magnet at the bottom of the cooling tank The magnetic induction intensity is 2T.

[0035] The transmission electron microscope picture of the above-mentioned alnico magnet after directional solidification and crystallization, that is, the TEM picture is as follows Figure 4 As shown, it can be seen from the figure that the ...

Embodiment 2

[0037] use Figure 1 to Figure 3The device for implementing the method of directional solidification and crystallization of metal alloy magnets shown in the figure is to carry out directional solidification and crystallization of a bar-shaped iron-chromium alloy magnet with a diameter of 8 mm and a length of 200 mm. The cooling body is liquid cooling water, the distance from the induction coil to the liquid surface of the cooling water is 40mm, the magnetic induction of the transverse magnet on the periphery of the induction coil is 2T, and the magnetic induction of the longitudinal magnet at the bottom of the cooling tank The strength is 2T.

[0038] The TEM image of the above iron-chromium alloy magnet after directional solidification and crystallization is similar to Figure 4 As shown, compared with the existing technology, after the directional solidification and crystallization of the device, the grain orientation of the iron-chromium alloy magnet is promoted, the degre...

Embodiment 3

[0040] use Figure 1 to Figure 3 The device for implementing the method of directional solidification and crystallization of metal alloy magnets shown in the figure is to carry out directional solidification and crystallization of rod-shaped nickel-niobium alloy magnets with a diameter of 6 mm and a length of 300 mm. The cooling body is liquid cooling water, the distance from the induction coil to the cooling water surface is 70mm, the magnetic induction of the transverse magnet on the periphery of the induction coil is 2T, and the magnetic induction of the longitudinal magnet at the bottom of the cooling tank The strength is 2T.

[0041] The TEM image of the above nickel-niobium alloy magnet after directional solidification and crystallization is similar to Figure 4 As shown, compared with the existing technology, after the directional solidification and crystallization of the device, the grain orientation of the nickel-niobium alloy magnet is promoted, the crystal orientat...

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Abstract

The invention discloses a directional solidifying crystallization method of a metal alloy magnet and a device for implementing the same. The method specifically comprises the following steps: enabling the bottom end of the metal alloy magnet to be contacted with a cooling liquid surface, and heating the metal alloy magnet on the cooling liquid surface by high-frequency induction heating equipment; allowing the metal alloy magnet to enter cooling liquid at a steady rate along the fixed movement direction for solidifying crystallization; and applying a constant longitudinal magnetic field to the metal alloy magnet entering the cooling liquid in the cooling liquid, wherein, the direction of the longitudinal magnetic field is parallel to the movement direction of the metal alloy magnet. Compared with the prior art, the invention has the advantages of promoting grain orientation of the metal alloy magnet, improving crystallization orientation degree and enhancing anisotropy. In addition, the preferred method of the invention overcomes the problems of gravity segregation of alloy melt and too small and uncontrolled temperature gradient in the prior art.

Description

technical field [0001] The invention relates to the technical field of magnetic material preparation, in particular to a method for directional solidification and crystallization of a metal alloy magnet and a device for implementing the method. Background technique [0002] Among magnetic materials, high-performance magnetic materials have become the research focus of scientific and technological workers in various countries because of their wide application value. [0003] Directional solidification crystallization is one of the core factors to improve magnetic properties. At present, countries around the world often use out-of-furnace crystallization method, power reduction method and power reduction method to prepare directionally solidified metal alloy magnet materials. [0004] The out-of-furnace crystallization method is to pour molten metal alloy liquid into a mold whose top is covered with exothermic agent and cooled at the bottom, so that the casting is solidified f...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22D27/02B22D27/04
Inventor 宋振纶胡方勤汪元亮张阳明
Owner NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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