Ceramic capacitor dielectric material
A technology of ceramic capacitors and ceramic dielectrics, applied in the direction of fixed capacitor dielectrics and components of fixed capacitors, etc., can solve the problems of high price, unfavorable enterprise development, and high cost of MLCC materials, and achieve excellent dielectric properties and material costs.
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[0011] 1. Preparation of glass flux: 5-10wt% Al 2 o 3 , 10-20 wt% SiO 2 , 15-25 wt% ZnO, 20-35 wt% CuO, 30-45 wt% V 2 o 5 Weigh each oxide separately, mix them in a ball mill, add deionized water according to the ratio of powder: water = 1: (1-1.5), and the ball milling time is 15-25 hours. After the ball milling is evenly mixed, dry, Pulverize, melt at 1150°C-1300°C for 1-3 hours, then pour into water to quench, and obtain the glass flux (glass powder) of the present invention after ultra-fine grinding, filtration and drying.
[0012] 2. According to the composition, the main component is barium zinc titanate of 85-92wt%, 1-4wt% of SrO, and 0.5-1.5wt% of Y 2 o 3 , 1~4 wt% Nb 2 o 5 , 0.1~0.4 wt% MnO 2 , 0.3~1.5 wt% of R 2 o 3 , R is at least one of La, Ce, Nd, Sm, 3~10wt% glass flux, weigh various materials, mix them in an ultrafine mill for ultrafine grinding, and the average particle size of the powder is required It is better to be smaller than 0.7 micron; then i...
Embodiment
[0014] (1) To analyze pure Al 2 o 3 , SiO 2 , ZnO, CuO, V 2 o 5 As the raw material, according to the composition ratio in Table 1, according to the glass powder preparation process described in 1 of the Summary of the Invention, the glass powder is obtained after the processes of ball milling, drying, melting, quenching, crushing, filtering, drying and the like.
[0015] (2) According to the composition in Table 2, the main material is analytically pure Ba synthesized by the oxalate method 1-x Zn x TiO 3 (0.01≤x≤0.06), add analytically pure SrO, Y 2 o 3 , Nb 2 o 5 , MnO 2 , R 2 o 3 (R is at least one of La, Ce, Nd, and Sm) and the glass powder described in (1), adding deionized water in a ball mill for ultra-fine pulverization, and drying to obtain the ceramic dielectric material of the present invention powder.
[0016] (3) The process of preparing capacitor samples: add PVA-based binder to the ceramic dielectric material described in (2) to granulate, apply a ...
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