Short-process degumming method for apocynum bast fiber
A degumming method and leather fiber technology, applied in the direction of producing bast fiber by chemical method, can solve the problems of high labor intensity, low efficiency, heavy pollution, etc., and achieve the effect of reducing labor intensity, reducing production cost, and reducing sewage discharge
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Embodiment 1
[0013] Put hydrogen peroxide with a concentration of 50g / L, penetrant JFC (commercially available) with a concentration of 1g / L, and sodium tripolyphosphate with a concentration of 10g / L in water, stir evenly, and prepare a loose solution, and then mix the hemp of Apocynum The skin is immersed in the loosening solution, the bath ratio is 1:15 (weight ratio), the temperature is raised to 100°C, and the skin is kept warm for 40 minutes to loosen;
[0014] Then add 30g / L sodium hydroxide to the treatment bath after loosening, keep the temperature at 80°C for 60min to carry out refining and boiling;
[0015] The degummed apocynum bast fiber can be obtained by putting the boiled hemp bark into the prepared washing solution with pH 6, and washing at 75°C for 25 minutes.
Embodiment 2
[0017] Sodium hypochlorite that concentration is 30g / L, concentration is that 3g / L penetrant JFC (commercially available) and concentration are 5g / L sodium tripolyphosphate is placed in water, stir evenly, be mixed with loose solution, then the hemp of Apocynum The skin is immersed in the loosening solution, the bath ratio is 1:10 (weight ratio), the temperature is raised to 90°C, and the skin is kept warm for 50 minutes to loosen;
[0018] Add 15g / L potassium hydroxide to the treatment bath after loosening, heat at 85°C for 15min for refining;
[0019] Put the boiled hemp bark in the prepared washing liquid with pH 5, wash at 80°C for 15 minutes, and then obtain the degummed apocynum bast fiber.
Embodiment 3
[0021] The concentration is 55g / L hydrogen peroxide, concentration is 5g / L penetrant T (commercially available) and concentration is the sodium silicate of 8g / L and is placed in water, stirs evenly, is mixed with loose solution, then the hemp husk of Apocynum apocynum Immerse in the loosening solution, the bath ratio is 1:20 (weight ratio), heat up to 75°C, keep warm for 90min to loosen;
[0022] Then add 35g / L sodium hydroxide to the treatment bath after loosening, keep the temperature at 75°C for 80min for refining and boiling;
[0023] The degummed apocynum bast fiber can be obtained by placing the boiled hemp bark in the prepared washing liquid with pH 5.5 at a temperature of 75°C for 20 minutes.
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