Zr-based amorphous alloy and preparation method thereof
A zirconium-based amorphous alloy and amorphous alloy technology, applied in the field of amorphous alloys and their preparation, can solve the problems of high purity requirements of raw materials, harsh preparation conditions, poor processing performance, etc., achieve excellent machinability, increase manufacturing The effect of slag function and excellent plastic deformation performance
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[0014] The invention provides a method for preparing a zirconium-based amorphous alloy, which comprises melting and cooling an amorphous alloy raw material in a protective gas atmosphere or vacuum condition, wherein the amorphous alloy raw material is formed according to the general formula (Zr x Al y Cu z Ni 1-x-y-z ) 100-a-b sc a Y b In the formula, x, y, z are atomic percentages, and a is the molar ratio of elements; where 0.45≤x≤0.60, 0.08≤y≤0.12, 0.25≤z≤0.35; 0<a≤5, 0≤b <0.1.
[0015] In the preparation method of the zirconium-based amorphous alloy provided by the present invention, a small amount of impurities contained in the amorphous alloy raw material have no effect on the smelting of the amorphous alloy. Based on the total amount of the zirconium-based amorphous alloy, the impurities The content may be 5 atomic % or less. The higher the purity of the various amorphous alloy raw materials used to prepare the zirconium-based amorphous alloy of the present inven...
Embodiment 1
[0022] This example illustrates the zirconium-based amorphous alloy provided by the present invention and its preparation method.
[0023] The various amorphous alloy raw materials with a purity of 95.5% by weight are dropped into an electric arc melting furnace (Shenyang Scientific Instrument Factory), the electric arc melting furnace is evacuated (the degree of vacuum is 5 Pa), and then the argon with a purity of 99.9% by volume is introduced. Gas is used as a protective gas, under the condition of 1300 ℃, smelting for 3 minutes, so that the amorphous alloy raw material is fully melted. The types and amounts of various amorphous alloy raw materials are 50.44 atomic % of Zr, 9.7 atomic % of Al, 29.585 atomic % of Cu, 7.275 atomic % of Ni, and 3 atomic % of Sc.
[0024] The molten alloy samples were then cast into copper molds by gravity casting, and 3 A cooling rate of K / s was used for cooling in a water-cooled copper mold to form a zirconium-based amorphous alloy sample A1 ...
Embodiment 2
[0034] Prepare zirconium-based amorphous alloy according to the method of Example 1, the difference is that the types and amounts of each amorphous alloy raw material are 51.74 atomic % of Zr, 9.95 atomic % of Al, 30.3475 atomic % of Cu, 7.4625 atomic % of Ni, 0.5 atomic % Sc.
[0035] Finally, an amorphous alloy sample A2 was obtained. Elemental analysis shows that the composition of the zirconium-based amorphous alloy sample A2 is (Zr 0.52 Al 0.10 Cu 0.305 Ni 0.075 ) 99.5 sc 0.5 .
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