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A kind of dyeing method of pokeweed ultrasonic extraction pigment to real silk fabric

A technology for silk fabrics and dyeing methods, applied in the field of pokeweed ultrasonic extraction of pigments for dyeing silk fabrics, can solve problems such as human health hazards, environmental pollution, stimulation, etc., achieve good reproducibility, simple extraction process, and color gain uniform effect

Inactive Publication Date: 2016-01-13
菲诺染料化工(无锡)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Synthetic dyes will cause great pollution to the environment during the production and use of textiles. Some synthetic dyes can also stimulate the human body, and even cause carcinogenic and teratogenic reactions, which are extremely harmful to human health.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] The present invention adopts ultrasonic wave to extract Phytaceae pigment to crepe de chine silk fabric (64g / m 2 ), the specific process steps are as follows:

[0022] (1) Extraction of pigment: get 40 parts of pokeweed berries, 60 parts of deionized water, mash the pokeweed berries with a glass rod, ultrasonicate for 20 minutes at a power of 500w on an ultrasonic cell pulverizer, filter twice with filter paper, Obtain pokeweed pigment solution;

[0023] (2) Preparation of dye solution: the amount of pigment solution is 10%, the bath ratio is 1:20, and the pH is adjusted to be 2;

[0024] (3) Dyeing of real silk fabrics: put the real silk fabrics into the dye liquor, dye in a oscillating water bath, set the temperature at 35°C, dyeing time is 30min, and dry at 70°C after dyeing;

[0025] The color of the dyed silk fabric is rose red, the K / S value is 1.3940; the dry rubbing fastness is 3-4, the wet rubbing fastness is 3; the fading fastness is 4, and the staining fast...

Embodiment 2

[0027] The present invention adopts ultrasonic wave to extract Phytaceae pigment to crepe de chine silk fabric (64g / m 2 ), the specific process steps are as follows:

[0028] (1) Extraction of pigment: get 45 parts of pokeweed stems, 55 parts of deionized water, cut pokeweed bark into pieces with scissors, and after ultrasonic cell pulverization with 600w power for 30min, filter paper twice to obtain pokeweed Lumin solution;

[0029] (2) Preparation of the dye solution: the dosage of Phytophthora pigment solution is 15%, the bath ratio is 1:20, and the pH is adjusted to be 4;

[0030] (3) Dyeing of real silk fabrics: put the real silk fabrics into the dye liquor, dye them in a oscillating water bath, set the temperature at 80°C, dye them for 45 minutes, and dry them at 70°C after dyeing;

[0031] The color of the silk fabric after dyeing is gray-green, the K / S value is 5.1170; the dry rubbing fastness is 4-5, the wet rubbing fastness is 3; the fading fastness is 3, and the s...

Embodiment 3

[0033] The present invention adopts ultrasonic wave to extract Phytaceae pigment to crepe de chine silk fabric (64g / m 2 ), the specific process steps are as follows:

[0034] (1) Extraction of pigment: get 50 parts of pokeweed leaves, 50 parts of deionized water, after cutting pokeweed leaves with scissors, after ultrasonic cell pulverization instrument 800w power ultrasonic 25min, filter paper filtration twice, obtain the pokeweed Lumin solution;

[0035] (2) Preparation of dyeing solution: the pigment dosage of pokeweed solution is 10%, the bath ratio is 1:20, and the pH is adjusted to be 6;

[0036] (3) Dyeing of real silk fabrics: put the real silk fabrics into the dye liquor, dye in a oscillating water bath, set the temperature at 40°C, dyeing time is 60min, and dry at 80°C after dyeing;

[0037] The color of the silk fabric after dyeing is lemon yellow, the K / S value is 1.394; the dry rubbing fastness is 4-5, the wet rubbing fastness is 3-4; the fading fastness is 3-4,...

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Abstract

The invention relates to a method for dyeing real silk fabrics by extracting pigment from phytolacca by ultrasonic technology, belonging to the technical field of textile chemistry. The method is characterized by extracting natural pigment from berries, stems or leaves of phytolacca by ultrasonic technology and using the natural pigment for dyeing the real silk fabrics. The method has the following beneficial effects: the extraction process is simple and environment-friendly; the real silk fabrics can be dyed into rose red, lemon yellow, grayish green and the like by changing the dyeing temperature and the pH value of the dye bath; and the dyed fabrics have uniform color, bright color, good color depth and excellent color fastness.

Description

technical field [0001] The invention relates to a method for dyeing real silk fabrics by ultrasonically extracting pigments from pokeweed and belongs to the technical field of textile chemistry. Background technique [0002] Synthetic dyes will cause great pollution to the environment during the production and use of textiles. Some synthetic dyes can also stimulate the human body, and even cause carcinogenic and teratogenic reactions, which are extremely harmful to human health. Dyeing with natural dyes can not only reduce the harm of dyes to the human body, make full use of natural renewable resources, but also greatly reduce the toxicity of dyeing wastewater, which is conducive to reducing the burden of sewage treatment and protecting the environment. [0003] With the increasingly prominent environmental problems, the reduction of renewable resources, and the continuous increase of population, the development and research of natural dye planting, production, processing an...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P3/04D06P1/34C09B61/00
Inventor 王潮霞卜广玖张冬梁建升
Owner 菲诺染料化工(无锡)有限公司