Gallium nitride based light-emitting diode (LED) epitaxial wafer and growth method thereof
An LED epitaxial wafer, GaN-based technology, applied in electrical components, circuits, semiconductor devices, etc., can solve the problems of dielectric melting, deterioration of LED performance parameters, leakage and other problems
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[0024] Example 1
[0025] 1. Put the (0001) crystal orientation sapphire substrate into the reaction chamber, and then in H 2 In the environment, the temperature is raised to 1050°C and stabilized for 10 minutes, and the substrate is purified at high temperature.
[0026] 2. Cool down to 530°C to grow a low-temperature GaN-based buffer layer with a thickness of 20nm.
[0027] 3. The temperature is raised to 1100°C to grow non-doped gallium nitride with a thickness of 1 μm.
[0028] 4. Growth of n-type gallium nitride with a thickness of 1.5 μm at 1100°C.
[0029] 5. In N 2 The multi-quantum well layer is grown for 10 cycles in the environment, GaN barrier layer: thickness is 20nm, growth temperature is 850℃; InGaN well layer: thickness is 2nm, growth temperature is 810℃.
[0030] 6. Raise temperature to 960℃ to grow p-type Al with a thickness of 30nm 0.15 Ga 0.85 N layer.
[0031] 7. Grow p-type gallium nitride with a thickness of 150 nm at 940°C.
[0032] 8. Grow low-doped p-type In with ...
Example Embodiment
[0035] Example 2
[0036] Growth using MOCVD method: Except for step 8, the other steps are as shown in Example 1. And the 8th step is:
[0037] 8. Grow low-doped n-type In with a thickness of 2nm at 810℃ 0.1 Ga 0.9 N and 2nm highly doped n-type In 0.2 Ga 0.8 N electrode contact layer.
[0038] In this embodiment, 300×300μm made by standard chip technology 2 The chip with ITO as the transparent electrode has an ESD yield rate of 90% at 4000V.
Example Embodiment
[0039] Example 3
[0040] Use MOCVD method to grow.
[0041] 1. Put the (0001) crystal orientation sapphire substrate into the reaction chamber, and then in H 2 In the environment, the temperature is raised to 1050°C and stabilized for 10 minutes, and the substrate is purified at high temperature.
[0042] 2. Cool down to 530°C to grow a low-temperature GaN-based buffer layer with a thickness of 20nm.
[0043] 3. The temperature is raised to 1100°C to grow undoped gallium nitride with a thickness of 1.5 μm.
[0044] 4. Grow n-type gallium nitride with a thickness of 2 μm at 1100°C.
[0045] 5. In N 2 A multi-quantum well layer is grown for 5 cycles in the environment, GaN barrier layer: thickness is 20nm, growth temperature is 850°C; InGaN well layer: thickness is 1.6nm, growth temperature is 810°C.
[0046] 6. Raise the temperature to 960℃ to grow p-type Al with a thickness of 30nm 0.15 Ga 0.85 N layer.
[0047] 7. Grow p-type gallium nitride with a thickness of 150 nm at 940°C.
[0048] 8...
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