Micron semisphere composed of silver nano-flakes as well as preparation method and use thereof
A technology of silver nanosheets and microhemispheres, applied in the field of microhemispheres and preparation, can solve the problems of inability to prepare, low sensitivity for detecting trace organics, restricting the detection range, etc., and achieves the effect of scientific preparation method
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Embodiment 1
[0026] The concrete steps of preparation are:
[0027] Step 1, uniformly mix silver nitrate aqueous solution with a concentration of 2g / L and citric acid aqueous solution with a concentration of 8g / L according to the volume ratio of 0.8:1.2 to obtain an electrolyte solution.
[0028] Step 2, put the conductive substrate as the cathode and the graphite sheet as the anode in the electrolyte, and the current density is 0.1mA / cm 2 Electrodeposition under constant current for 180min; wherein, the conductive substrate is conductive glass. made approximately figure 1 as shown in a~f, and as figure 2 The silver nanosheets shown in the curves are composed of micron hemispheres.
Embodiment 2
[0030] The concrete steps of preparation are:
[0031]Step 1, uniformly mix silver nitrate aqueous solution with a concentration of 10 g / L and citric acid aqueous solution with a concentration of 42 g / L according to a volume ratio of 0.9:1.1 to obtain an electrolyte solution.
[0032] Step 2, put the conductive substrate as the cathode and the graphite sheet as the anode in the electrolyte, and the current density is 0.3mA / cm 2 Electrodeposition under constant current for 140min; wherein, the conductive substrate is conductive glass. made approximately figure 1 as shown in a~f, and as figure 2 The silver nanosheets shown in the curves are composed of micron hemispheres.
Embodiment 3
[0034] The concrete steps of preparation are:
[0035] Step 1, uniformly mix silver nitrate aqueous solution with a concentration of 17g / L and citric acid aqueous solution with a concentration of 76g / L according to a volume ratio of 1:1 to obtain an electrolyte solution.
[0036] Step 2, place the conductive substrate as the cathode and the graphite sheet as the anode in the electrolyte, and place it at a current density of 0.5mA / cm 2 Electrodeposition under constant current for 90min; wherein, the conductive substrate is conductive glass. made as figure 1 as shown in a~f, and as figure 2 The silver nanosheets shown in the curves are composed of micron hemispheres.
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