Preparation method of phenolic resin microballoons and method for preparing phenolic resin-based carbon spheres by use of preparation method
The technology of phenolic resin and microspheres is applied in the field of preparation of resin microspheres and carbon spheres, which can solve the problems of high cost, complicated preparation method, difficult control of the diameter of microspheres, etc. simple craftsmanship
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[0010] Specific embodiment 1: The preparation method of phenolic resin microspheres in this embodiment is carried out according to the following steps: Step 1. According to the molar ratio of resorcinol and phenol of 1:0-9, resorcinol and formaldehyde The molar ratio of resorcinol to sodium carbonate is 1:1.2~2.7, the molar ratio of resorcinol to sodium carbonate is 1:0~0.002, the molar ratio of resorcinol to sodium bicarbonate is 1:0~0.002, and the molar ratio of resorcinol to sodium bicarbonate is 1:0~0.002. The molar ratio of water is 1:16-60. Mix resorcinol, phenol, formaldehyde, sodium carbonate, sodium bicarbonate and water, and stir for 10-30min under the condition of 15-30r / min to obtain a reaction solution; step 2. Place the reaction solution of step 1 in an oil bath, stir at 20-30 r / min while heating to 70-150°C and keep it for 4-6 hours to obtain a phenolic resin microsphere suspension; step 3. The phenolic resin microsphere suspension is suction filtered, washed wit...
Example Embodiment
[0012] Specific embodiment two: this embodiment is different from specific embodiment one in that the molar ratio of resorcinol to phenol in step one is 1:0.4-6. The other steps and parameters are the same as in the first embodiment.
Example Embodiment
[0013] Specific embodiment three: This embodiment is different from specific embodiment one in that the molar ratio of resorcinol to phenol in step one is 1:5. The other steps and parameters are the same as in the first embodiment.
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