High-temperature resistant alkyd paint
A technology of high temperature resistant and alkyd paint, applied in the field of temperature resistant paint, can solve the problems of baking yellowing, yellowing, chalking, etc., and achieve the effects of short production cycle, reduced reaction time and energy saving
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Embodiment 1
[0019] Embodiment 1: (by weight)
[0020] High temperature resistant alkyd resin, prepared from the following raw materials in parts by weight:
[0021] Trimethylolpropane 7.3%, neopentyl glycol 9.3%, isophthalic acid 12.8%, castor oil 17.6%, trimellitic anhydride 7.3%, xylene 5%, tolyl butanone (10:1) mixed solvent 40.7%.
[0022] The preparation method of high temperature resistant alkyd resin is as follows:
[0023] (1) Put trimethylolpropane, neopentyl glycol, and isophthalic acid in sequence in the reaction kettle, heat it to 150°C and keep it warm until the acid value is less than or equal to 10mgKOH / g; obtain material A;
[0024] (2) Cool the material A to below 120°C, put in castor oil, trimellitic anhydride, and xylene, and carry out reflux reaction. After the temperature reaches 160°C, it starts to heat up at a rate of 10°C / h, and then rises to 200°C for heat preservation until the acid value ≤15mgKOH / g; obtain material B;
[0025] (3) Lower the temperature of mat...
Embodiment 2
[0029] Embodiment 2: (by weight ratio)
[0030] High temperature resistant alkyd resin, prepared from the following raw materials in parts by weight:
[0031] Trimethylolpropane 6.3%, neopentyl glycol 11.3%, isophthalic acid 11.8%, castor oil 22.6%, trimellitic anhydride 9.3%, xylene 2.2%, tolyl butanone (10:1) mixed solvent 36.5%.
[0032] The preparation method of high temperature resistant alkyd resin is as follows:
[0033] (1) Put trimethylolpropane, neopentyl glycol, and isophthalic acid in sequence in the reactor, heat it to 170° C. and keep it warm until the acid value is less than or equal to 10 mgKOH / g; obtain material A;
[0034] (2) Cool the material A to below 120°C, put in castor oil, trimellitic anhydride, and xylene, and carry out reflux reaction. After the temperature reaches 160°C, it starts to heat up at a rate of 10°C / h, and then rises to 200°C for heat preservation until the acid value ≤15mgKOH / g; obtain material B;
[0035] (3) Lower the temperature of...
Embodiment 3
[0039] Embodiment 3: (by weight ratio)
[0040] High temperature resistant alkyd resin, prepared from the following raw materials in parts by weight:
[0041] Trimethylolpropane 5.3%, neopentyl glycol 13.3%, isophthalic acid 10.8%, castor oil 27.6%, trimellitic anhydride 11.3%, xylene 0%, tolyl butanone (10:1) mixed solvent 31.7%.
[0042] Preparation:
[0043] The preparation method of high temperature resistant alkyd resin is as follows:
[0044] (1) Put trimethylolpropane, neopentyl glycol, and isophthalic acid in sequence in the reactor, heat it to 180° C. and keep it warm until the acid value is ≤10 mgKOH / g; obtain material A;
[0045] (2) Cool the material A to below 120°C, put in castor oil, trimellitic anhydride, and xylene, and carry out reflux reaction. After the temperature reaches 160°C, it starts to heat up at a rate of 10°C / h, and then rises to 200°C for heat preservation until the acid value ≤15mgKOH / g; obtain material B;
[0046] (3) Lower the temperature o...
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