Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Dissolution technology of high alumina fly ash by method of sulphuric acid

A technology of high-alumina fly ash and sulfuric acid method, which is applied to the removal of alumina/hydroxide and solid waste, can solve the problems of iron and impurity removal, equipment corrosion, etc., and achieve corrosion and low cost , the effect of simple method

Active Publication Date: 2012-04-04
GUIYANG AL-MG DESIGN & RES INST
View PDF3 Cites 11 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage is that aluminum chloride solution is difficult to remove iron and impurities, hydrochloric acid is very corrosive to equipment at a temperature of 80-160 ° C, and some technical and material problems need to be further studied and solved

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Dissolution technology of high alumina fly ash by method of sulphuric acid
  • Dissolution technology of high alumina fly ash by method of sulphuric acid

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Embodiment 1 of the present invention: high-alumina fly ash sulfuric acid dissolution process, the high-alumina fly ash with a mass percentage content of 45% and dilute sulfuric acid with a mass percentage concentration of 35% adopt the alumina dissolution chemical reaction theory The ratio of the calculated amount to 1.0 is mixed to make the raw ore pulp A; the raw ore pulp A is sent into the dissolution device (the dissolution device includes a casing, a pressure cooker and a self-evaporator) through a dissolution feed pump at room temperature, and firstly use The steam heats the 1-3 level casing to 88°C (the inner tube of the casing is a lead alloy inner tube, and the outer tube is a stainless steel tube), and the raw ore slurry A is preheated through the 1-3 level casing, and the preheated The temperature of the raw pulp A reaches 85-87°C to obtain the preheated pulp B; then re-introduce steam to heat the casing to 150°C, so that the preheated pulp B is heated to 150...

Embodiment 2

[0020] Embodiment 2 of the present invention: High-alumina fly ash sulfuric acid dissolution process, the high-alumina fly ash with a mass percentage content of 40% and dilute sulfuric acid with a mass percentage concentration of 38% adopt the alumina dissolution chemical reaction theory The ratio of the calculated amount to 1.0 is mixed to make the raw ore pulp A; the raw ore pulp A is sent into the dissolution device (the dissolution device includes a casing, a pressure cooker and a self-evaporator) through a dissolution feed pump at room temperature, and firstly use The steam heats the 1-3 casing to 90°C (the inner tube of the casing is a lead alloy inner tube, and the outer casing is a stainless steel tube), and the raw ore slurry A is preheated through the 1-3 casing, and the preheated The temperature of the raw ore pulp A reaches 87°C to obtain the preheated ore pulp B; then re-introduce steam to heat the casing to 150°C, so that the preheated ore pulp B is heated to 150°...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a dissolution technology of high alumina fly ash by a method of sulphuric acid, comprising the following steps: mixing high alumina fly ash with dilute sulfuric acid in proportion to obtain an original pulp A; sending the original pulp A into a dissolution unit through a dissolution charging pump, preheating through grade 1-3 sleevings to obtain a preheat pulp B; heating the sleevings to heat the preheat pulp B to obtain a heating pulp C; sending the heating pulp C in a digester for carrying out insulation dissolution to obtain a dissolved pulp D under the conditions of insulation and pressure maintaining; and carrying out 3-level self-evaporation cooling on the dissolved pulp D, and then sending the cooled dissolved pulp D and an acid sludge washing liquor E into a dilution trap to obtain a mixed pulp F. According to the invention, alumina is dissolved out from the high alumina fly ash and enters in the solution, and the dissolution rate of alumina is 85-90 %, so that the preparation for subsequent production process is made; the high alumina fly ash is utilized reasonably, the cost is low, the advantage of economic rationality is achieved, and the problem of corrosion of devices in the dissolution process is solved.

Description

technical field [0001] The invention relates to the field of alumina industry, in particular to a high-aluminum fly ash dissolution process. Background technique [0002] At present, more than 70 million tons of alumina are produced every year in the world, and almost all alumina plants use bauxite as raw material. my country is the largest alumina producer in the world, with an annual output of about 30 million tons of alumina, accounting for about 40% of the world's total output. However, my country's bauxite resources are relatively poor. Bauxite reserves only account for about 6% of the world's total reserves. The ore grade is low. The ore type is mainly difficult to handle diaspore. , and the production cost is also higher. Due to the serious shortage of bauxite resources in our country, we can only rely on importing ore from abroad to solve the problem of raw materials. my country imports about 30 million tons of bauxite ore annually, accounting for about 50% of the d...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C01F7/02B09B3/00
Inventor 陈德
Owner GUIYANG AL-MG DESIGN & RES INST
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products