Novel application of licorice total saponin
A technology of total saponins and licorice, applied in the new application field of licorice total saponins, to achieve the effects of increasing serum DA content, improving intestinal sensitivity and inhibiting abdominal pain
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Embodiment 1
[0023] The preparation method of embodiment 1 total saponins of Glycyrrhizae
[0024] (1) Take licorice coarse powder, percolate with 20 times the amount of 95% ethanol, filter the percolate, concentrate under reduced pressure at 70°C to form a thick paste, stir and dissolve with heated water, and then use petroleum ether, ethyl acetate, water Saturated n-butanol extraction, the part obtained from ethyl acetate is the total flavonoids, and the n-butanol extract is used for later use.
[0025] (2) Take the filter residue obtained in step (1), percolate with 20 times the amount of 20% V / V ethanol, and after the percolation liquid is filtered, the extract is concentrated under reduced pressure at 60-70°C until it has no alcohol smell, and then saturated with n-butyl alcohol Alcohol extraction, the obtained extract is combined with the n-butanol extract obtained in step (1), after the n-butanol is recovered under reduced pressure, the residue is dissolved in water, centrifuged, th...
experiment example 1
[0030] Experimental example 1 Experimental study on the treatment of glacial acetic acid visceral hypersensitivity IBS disease model with total licorice saponins
[0031] 1.1 Materials and methods
[0032] 1.1.1 Drugs
[0033] 1.1.1.1 Test drug: total glycyrrhizin (prepared in Example 1).
[0034] 1.1.1.2 Positive drug: Trimebutin Tablets, produced by Tianjin Tanabe Pharmaceutical Co., Ltd., production batch number: 0905005, specification: 0.1g / tablet×20 tablets / box. During the experiment, distilled water was used to prepare a medicinal solution with a concentration of 2% (containing 0.02 g of trimebutin per milliliter) for subsequent use.
[0035] 1.1.1.3 Main reagents: 0.5% glacial acetic acid (volume fraction), 1.5% sodium pentobarbital, normal saline, liquid paraffin.
[0036] 1.1.2 Animals
[0037] SD rats, both male and female, weighing 200±20g, were provided by the Experimental Animal Research Center of Chengdu University of Traditional Chinese Medicine, license num...
experiment example 2
[0055] Experimental example 2 Experimental study on the treatment of mustard oil visceral hypersensitivity IBS disease model by total licorice saponins
[0056] 1.1 Materials and methods
[0057] 1.1.1 Drugs
[0058] 1.1.1.1 Test drug: total glycyrrhizin (prepared in Example 1).
[0059] 1.1.1.2 Positive drug: Trimebutin Tablets, produced by Tianjin Tanabe Pharmaceutical Co., Ltd., production batch number: 0905005, specification: 0.1g / tablet×20 tablets / box. During the experiment, distilled water was used to prepare a medicinal solution with a concentration of 2% (containing 0.02 g of trimebutin per milliliter) for subsequent use.
[0060] 1.1.1.3 Main reagents: 5% mustard oil (volume fraction), 1.5% sodium pentobarbital, normal saline, liquid paraffin.
[0061] 1.1.1.4 Animals
[0062] SD rats, both male and female, weighing 200±20g, were provided by the Experimental Animal Research Center of Chengdu University of Traditional Chinese Medicine, license number: 04-11, and we...
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