Regenerated animal micropowder protein cellulose fiber and preparation method thereof
A technology for cellulose fiber and regenerated protein, which is applied in the fields of cellulose/protein conjugated rayon, spinning solution preparation, wet spinning, etc. Cavity structure and other problems, to achieve the effect of better textile processing and wearing performance, lower density and comfortable wearing of regenerated animal micronized protein cellulose fibers
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Embodiment 1
[0033] Example 1 1.67dtex×38mm regenerated animal micronized protein viscose fiber
[0034] First, prepare animal micronized protein: add textile waste wool to 9wt% sodium hydroxide solution, bath ratio is 1:6, soak at 21℃ for 60 minutes, wash at 35℃, filter to remove impurities Afterwards, it is dried in a three-dimensional rotary oven at a drying temperature of 80°C, and then pre-crushed. The pre-crushed wool is added to 15.8wt% sodium hydroxide solution, the bath ratio is 1:11.5, and the temperature is 31°C Swell for 105 minutes, then grind it to an animal protein powder with an average particle size of 8.5 microns by a grinding pump. The ground animal protein powder is washed at a temperature of 41°C, and then dried at 71°C. The dried animal The protein powder is pulverized to an average particle size of 1.3 micrometers to obtain fine animal protein powder.
[0035] Preparation of animal micropowder protein viscose fiber: adding animal micropowder protein with an average parti...
Embodiment 2
[0037] Example 2 1.33dtex×38mm regenerated animal micronized protein viscose fiber
[0038] First, prepare animal micropowder protein: add pig hair to 11.5wt% sodium hydroxide solution, bath ratio of 1:8, soak at 23℃ for 80 minutes, wash at 38℃, filter to remove impurities A three-dimensional rotary oven is used for drying at a drying temperature of 83°C, and then pre-crushed. The pre-crushed pig hair is added to the 18.7wt% sodium hydroxide solution, the bath ratio is 1:14.5, and the temperature is 33°C Swell for 120 minutes, then grind it to an animal protein powder with an average particle size of 9.5 microns by a grinding pump. The ground animal protein powder is washed at a temperature of 43°C, and then dried at 72°C. The dried animal The protein powder is pulverized to an average particle size of 2.0 microns to obtain fine animal protein powder.
[0039] Preparation of animal micropowder protein viscose fiber: adding animal micropowder protein with an average particle size ...
Embodiment 3
[0041] Example 3 2.78dtex×51mm regenerated animal micronized protein viscose fiber
[0042] First, prepare animal micropowder protein: add feathers to 8.2wt% sodium hydroxide solution with a bath ratio of 1:5. After soaking at a temperature of 18℃ for 62 minutes, wash with water at a temperature of 33℃ and filter to remove impurities. Dry in a three-dimensional rotary oven at a drying temperature of 77.5°C, and then pre-crush, add the pre-crushed feathers to a 15wt% sodium hydroxide solution, bath ratio 1:10.5, and swell at 28°C for 105 minutes , And then grind to animal protein powder with a particle size of 8-10 microns by a grinding pump, wash the ground animal protein powder at a temperature of 38℃, and then dry it at 68℃. The dried animal protein powder It is pulverized to a particle size of 1 to 2.2 microns to obtain animal micropowder protein.
[0043] Preparation of animal micronized protein viscose fiber: Add animal micronized protein with an average particle diameter o...
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