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High heat-conductivity epoxy casting material for dry power transformer and preparation method thereof

A technology of epoxy casting and high thermal conductivity, which is applied in the field of high thermal conductivity epoxy castable and its preparation, can solve the problems such as the easy sedimentation of powder, and achieve the effect of reducing temperature rise

Inactive Publication Date: 2012-06-27
GUILIN UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The main difficulty in applying inorganic powders with higher thermal conductivity to castables for dry-type power transformers is that these powders with higher thermal conductivity generally have a higher density, for example, the density of alumina is 3.97g / cm 3 , the density of aluminum nitride is 3.26g / cm 3 , the castable powder is more likely to settle during the curing process

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0022] Castable formula: CYD127 epoxy resin 100kg; ethylene glycol glycidyl ether hydrolyzate 15kg; methyltetrahydrophthalic anhydride 85kg; accelerator DMP-300.25kg; iron oxide red 4kg; 300 mesh alumina powder 520kg .

[0023] Preparation:

[0024] (1) Put 100kg of CYD127 epoxy resin and 4kg of iron oxide red into the first thin-layer defoaming kettle, start stirring, and put in 260kg of 300-mesh alumina powder when the temperature rises to 80-90°C, stir evenly and decompress and degas Foaming, defoaming at 100-105°C and 100-200Pa until no bubbles are released to obtain component A;

[0025] (2) 85kg methyltetrahydrophthalic anhydride and 15kg ethylene glycol glycidyl ether hydrolyzate are dropped into the second thin-layer defoaming kettle, and 0.25kg accelerator DMP-30 is dropped into after starting stirring, and the temperature is raised to 80 Add 260kg of 300-mesh alumina powder at ~90°C, stir evenly, degas under reduced pressure, and defoam at 90-95°C and 100-200Pa unt...

Embodiment 2

[0029] Castable formula: DER383 epoxy resin 100kg; pyromellitic anhydride triethylene glycol ester 5kg; ethylene glycol glycidyl ether hydrolyzate 10kg; methyltetrahydrophthalic anhydride 85kg; accelerator DMP-300.23 kg; iron oxide green 5kg; 400 mesh alumina powder 510kg.

[0030] Preparation:

[0031] (1) Put 100kg of DER383 epoxy resin and 5kg of iron oxide green into the first thin-layer defoaming kettle, start stirring, put in 255kg of 400-mesh alumina powder when the temperature rises to 80-90°C, stir evenly, and decompress and degas Foaming, defoaming at 100-105°C and 100-200Pa until no bubbles are released to obtain component A;

[0032] (2) Methyltetrahydrophthalic anhydride, pyromellitic anhydride trimethylene glycol ester, and ethylene glycol glycidyl ether hydrolyzate are successively put into the second thin-layer defoaming kettle, and after stirring Put in the accelerator DMP-30, put in 255kg of 400-mesh alumina powder when the temperature rises to 80-90°C, sti...

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Abstract

The invention discloses a high heat-conductivity epoxy casting material for a dry power transformer and a preparation method thereof. Instead of silicon powder used in the prior art, the high heat-conductivity inorganic powder is used as padding, so that the coefficient of heat conductivity of the casting material is increased. The invention is characterized in that: 1) a toughening agent with higher hydroxyl content is selected, so that the impact resistance and the toughness of cured matters are improved while the acting force between the inorganic powder and the substrate resin molecules is increased; and 2) the formula of the casting material and the technical measures, such as a rubber mixing and de-foaming technology, are optimized, so that the easily sinking phenomenon of the high heat-conductivity inorganic powder caused by higher density is eliminated. The coefficient of heat conductivity of the obtained high heat-conductivity epoxy casting material can reach 1.1-1.3W / (m K); the impact resistance can reach 14-22kJ / m<2>; the difference between the density of the upper part of a workpiece and the density of the lower part of the workpiece is not more than + / -0.5%; the bending strength is 120-140MPa; the coefficient of linear expansion is 30-50*10<-6>K<-1>; the thermal deformation temperature is 105-120 DEG C; and the breakdown field strength is 26-30kV / mm.

Description

technical field [0001] The invention relates to a high thermal conductivity epoxy casting material for a dry-type power transformer and a preparation method thereof. Background technique [0002] Dry-type power transformers are widely used in urban and rural power distribution systems. At present, the insulation system of dry-type power transformer coils mainly has two insulation methods: casting type and resin impregnated type. For castable dry-type transformers, in order to reduce the linear expansion coefficient of the insulating layer, improve the heat transfer performance of the insulating layer, and improve the heat dissipation of the transformer, it is usually necessary to add a certain amount of inorganic powder to the castable. [0003] The inorganic powder added to the castable of the existing castable dry-type power transformer is relatively simple, mainly silicon micropowder or quartz powder. One of the advantages of microsilica powder is its low price, and anot...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B26/14
Inventor 饶保林李小萍
Owner GUILIN UNIVERSITY OF TECHNOLOGY
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