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Thick-wall bearing steel pipe drawing lubricating emulsifying oil and production method thereof

A technology of emulsified oil and oleic acid, which is applied in the direction of lubricating composition, petroleum industry, etc., can solve problems such as the surface finish of the drawn workpiece, the reduction of brightness, the adverse effects of heat treatment and annealing quality, and the impact on the service life of the mold, so as to improve the reduction Diameter ratio and radial drawing growth rate, good lubricity, and the effect of improving production efficiency

Inactive Publication Date: 2012-07-18
DALIAN SANDAAOKE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the lubricating emulsified oil for drawing thick-walled bearing steel pipes has the problems of poor cleaning performance and poor cooling effect, so that after many times of drawing, a large amount of metal powder adheres to the surface of the drawn tube and the edge of the hole core, resulting in two The friction coefficient between the two increases sharply, which not only reduces the surface finish and brightness of the drawn workpiece sharply, but also aggravates the wear on the mold and affects the service life of the mold; The quality problem of broken pipe due to local overheating of the mold
In addition, due to poor cleaning performance, it will have a negative impact on the quality of heat treatment and annealing in the subsequent process of drawing metal pipes

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Get raw material components, each raw material accounts for the percentage of total weight as follows:

[0024] Oleic acid 1~15%, barium petroleum sulfonate 1~8%, lead naphthenate 1~8%, chlorinated paraffin 10~20%, 2,6-di-tert-butyl-p-cresol (T501) 10~20 %, triethyl phosphate 1~4%, dibutyl phthalate 1~4%, zinc dialkyl dithiophosphate (T202) 1~6%, poly n-butyl vinyl ether (T601) 1 ~6% and transformer oil balance.

[0025] The sum of the mass of each raw material is 100%.

[0026] The production method is carried out according to the following steps: add the calculated amount of transformer oil into the reaction ax and heat it to 40~50°C, start the agitator and control the speed at 40 rpm, and then sequentially add the calculated amount of barium petroleum sulfonate, naphthene lead acid, oleic acid, chlorinated paraffin, triethyl phosphate, dibutyl phthalate, 2,6-di-tert-butyl p-cresol, zinc dialkyl dithiophosphate, poly-n-butyl vinyl Slowly add the ether into the reac...

Embodiment 2

[0028] 8% oleic acid, 5% barium petroleum sulfonate, 4% lead naphthenate, 15% chlorinated paraffin, 15% 2,6-di-tert-butyl p-cresol (T501), 2% triethyl phosphate, ortho Dibutyl phthalate 2%, zinc dialkyldithiophosphate (T202) 4%, poly-n-butyl vinyl ether (T601) 3%, and the balance of transformer oil.

[0029] The sum of the mass of each raw material is 100%.

[0030] Production method is with embodiment 1.

[0031] When in use, add water to dilute the products of Examples 1 and 2, prepare an emulsion with a concentration of 8%, and apply it to the drawing of thick-walled bearing steel pipes until the blank material is drawn to the required diameter, without broken pipes, and the surface The smoothness and brightness meet the requirements of national standards.

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PUM

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Abstract

The invention discloses thick-wall bearing steel pipe drawing lubricating emulsifying oil, which consists of the following raw material components in percentage by mass: 1-15 percent of oleic acid, 1-8 percent of barium mahogany sulfonate, 1-8 percent of lead naphthenate, 10-20 percent of chlorinated paraffin, 10-20 percent of 2,6-butylated hydroxytoluene, 1-4 percent of triethyl phosphate, 1-4 percent of dibutyl phthalate, 1-6 percent of zinc dialkyl dithiophosphate, 1-6 percent of polyvinyl butyl ether and the balance transformer oil. A production method of the emulsifying oil comprises the following steps of: adding the transformer oil into a reaction kettle, and heating to 40-50 DEG C; starting a stirrer and controlling the rotating speed at 40 revolutions per minute; slowly and sequentially adding barium mahogany sulfonate, lead naphthenate, oleic acid, chlorinated paraffin, triethyl phosphate, dibutyl phthalate, T501, T202 and T601 into the reaction kettle, wherein a next raw material is added till a previous raw material is fully dissolved by stirring; after all raw materials are dissolved, continually stirring for 1 hour; and discharging and packaging.

Description

technical field [0001] The invention relates to a lubricating emulsified oil for drawing process and its production method, in particular to a drawing lubrication for thick-walled bearing steel pipes which can prevent local overheating of the drawn metal pipe, oxidative discoloration, and ensure the surface finish and brightness of the finished product. Emulsified oil and production method. Background technique [0002] The drawing process is a typical metal processing method. It is a plastic processing process that reduces the cross-sectional area of ​​the metal processing material through the die hole core under the action of drawing to obtain a high-precision, high-gloss wire or pipe. During the drawing process, due to the large amount of metal deformation and the continuous generation of new friction surfaces, lubricating emulsified oil is required to lubricate and cool the metal material and mold. Lubricating emulsified oil plays a vital role in such a huge extrusion a...

Claims

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Application Information

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IPC IPC(8): C10M169/00C10N40/24C10N30/04C10N30/16
Inventor 潘德顺孙倩倩朱咏红陈忠孝
Owner DALIAN SANDAAOKE CHEM
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