Preparation method for solid high temperature resistant acidic mannase
A technology of mannanase and preparation method, which is applied in the preparation field of solid high temperature resistant acid mannanase, can solve the problems of unseen fermentation production, extraction and manufacturing, etc.
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Embodiment 1
[0021] Soaking: Mix the rhizopus solid fermented koji material with water at a ratio of 1:10, adjust the pH of the soaking water to 4.5 with acetic acid, and stir for 2.6 hours;
[0022] Centrifugation: Centrifuge in a three-legged centrifuge for 15 minutes at a speed of 800 rpm, and take the supernatant after centrifugation;
[0023] Plate and frame filtration: add 10% diatomaceous earth, filter with a plate and frame filter to obtain the filtrate;
[0024] Ultrafiltration concentration: membrane molecular weight 10000, concentrated to 1 / 10 of the filtrate volume;
[0025] Spray drying: According to the ratio of concentrated solution: corn starch: sodium carboxymethyl cellulose = 1:0.2:0.03, stir evenly, the inlet air temperature of spray drying: 180°C, the outlet air temperature: 80°C, the final moisture content of the material: 5.9%.
[0026] source of material
[0027] Koji material: fermented from Rhizopus solid
[0028] Detection method used in the present invention-...
Embodiment 2
[0107] Soaking: Mix the rhizopus solid fermented koji material with water at a ratio of 1:16, adjust the pH of the soaking water to 4.5 with acetic acid, and stir for 2 hours;
[0108] Centrifugation: Centrifuge in a three-legged centrifuge for 12 minutes at a speed of 1000 rpm, and take the supernatant after centrifugation;
[0109] Plate and frame filtration: add 8% diatomaceous earth, filter with a plate and frame filter to obtain the filtrate;
[0110] Ultrafiltration concentration: membrane molecular weight 10000, concentrated to 1 / 12 of the filtrate volume;
[0111] Spray drying: According to the ratio of concentrated liquid: corn starch: sodium carboxymethyl cellulose = 1:0.2:0.03, stir evenly, the inlet air temperature of spray drying: 170°C, the outlet air temperature: 76°C, the final moisture content of the material: 6.2%.
Embodiment 3
[0113] Soaking: Mix the rhizopus solid fermented koji material with water at a ratio of 1:8, adjust the pH of the soaking water to 4.5 with acetic acid, and stir for 3 hours;
[0114]Centrifugation: Centrifuge in a three-legged centrifuge for 12 minutes at a speed of 1200 rpm, and take the supernatant after centrifugation;
[0115] Plate and frame filtration: add 7% diatomaceous earth, filter with a plate and frame filter to obtain the filtrate;
[0116] Ultrafiltration concentration: membrane molecular weight 10000, concentrated to 1 / 8 of the filtrate volume;
[0117] Spray drying: According to the ratio of concentrated solution: corn starch: sodium carboxymethyl cellulose = 1:0.2:0.03, stir evenly, the inlet air temperature of spray drying: 160°C, the outlet air temperature: 70°C, the final moisture content of the material: 7.0%.
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