Method for preparing polyester staple fibers by using waste polyester raw material
A polyester staple fiber and polyester technology, which is applied in the field of polyester staple fiber preparation by using waste polyester raw materials, can solve the problems of low processing efficiency, molecular weight reduction, high-new material ratio, etc., so as to improve processing efficiency, avoid gel phenomenon, and ensure The effect of linearity
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[0017] Example 1:
[0018] The waste polyester raw material used is waste pure polyester textiles (intrinsic viscosity 0.5g / dl). The following process conditions are used to prepare recycled polyester fiber:
[0019] (1) Preparation of raw materials: cleaning waste polyester textiles to remove stains, and the cleaning conditions are: synthetic detergent 5g / l, sodium tripolyphosphate 5g / l, caustic soda 0.8g / l, temperature 90°C. The washed waste polyester textiles are dried in a hot-air dryer for 5 hours. After the moisture content is reduced to 0.1%, the waste polyester raw materials are compressed in a semi-molten state at 235° C. to prepare spherical pellets.
[0020] (2) Melt preparation and spinning: transport the pellets prepared in step (1) to a drying device for drying at 120°C for 30 minutes, and then drying at 140°C for 6 hours. After drying, the moisture content is 30 ppm, and then press the pellets Add 0.5% of the mass of 1,4-phenylbisoxazoline (1,4-PBO) and carbonyl bis(...
Example Embodiment
[0022] Example 2:
[0023] The waste polyester raw material used is the waste yarn (intrinsic viscosity 0.6g / dl) produced during the spinning process of polyester. The following process conditions are used to prepare recycled polyester fiber:
[0024] (1) Preparation of raw materials: cleaning waste polyester textiles to remove stains, and the cleaning conditions are: synthetic detergent 5g / l, sodium tripolyphosphate 5g / l, caustic soda 0.8g / l, temperature 90°C. The washed waste polyester textiles are dried in a hot-air dryer for 5 hours. After the moisture content is reduced to 0.1%, the waste polyester raw materials are compressed in a semi-molten state at 235° C. to prepare spherical pellets.
[0025] (2) Melt preparation and spinning: transport the pellets prepared in step (1) to a drying device for drying at 140°C for 10 minutes, and then drying at 170°C for 3 hours. After drying, the moisture content is 40ppm, and then according to the pellet quality Add 3% of the 1,4-phenylbi...
Example Embodiment
[0026] Example 3:
[0027] The waste polyester raw material used is waste pure polyester textiles (intrinsic viscosity 0.52g / dl). The following process conditions are used to prepare recycled polyester fiber:
[0028] (1) Preparation of raw materials: cleaning waste polyester textiles to remove stains, and the cleaning conditions are: synthetic detergent 5g / l, sodium tripolyphosphate 5g / l, caustic soda 0.8g / l, temperature 90°C. The washed waste polyester textiles are dried in a hot-air dryer for 5 hours. After the moisture content is reduced to 0.1%, the waste polyester raw materials are compressed in a semi-molten state at 235° C. to prepare spherical pellets.
[0029] (2) Melt preparation and spinning: transport the pellets prepared in step (1) to a drying device for drying at 130°C for 20 minutes, and then drying at 160°C for 4 hours. After drying, the moisture content is 45 ppm, and then press the pellets Add 2.5% of the mass of carbonyl bis(1,-caprolactam) (CBC) polyester chai...
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