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Application of macroporous adsorption resin to cigarettes

A technology of pore adsorption and resin, which is applied in the field of cigarette harm reduction additive materials, can solve the problems of high cost, complicated material preparation process, and not being widely used, and achieve the effect of improving adsorption rate and large specific surface area

Inactive Publication Date: 2012-07-25
ZHENGZHOU TOBACCO RES INST OF CNTC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] To sum up, some explorations and researches have been carried out at home and abroad to reduce the release of phenol in cigarette smoke, but these technologies have poor selective adsorption capacity for phenol in cigarette smoke, and at the same time, the material preparation process is complicated and the cost is high , have not been widely used

Method used

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  • Application of macroporous adsorption resin to cigarettes
  • Application of macroporous adsorption resin to cigarettes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Prepare the oil phase first, the composition is 6ml styrene, 2ml divinylbenzene, 5ml toluene, 0.2g benzoyl peroxide BPO, and then configure the water phase, the composition is 80 ml water, 0.5g sodium chloride and 2 g polyethylene alcohol. Under stirring, the water phase was added into the oil phase, then the temperature was raised to 80° C., and the reaction was carried out for 12 hours. The obtained spherical product was extracted with ethanol for 24 hours to obtain the macroporous adsorption resin 1.

[0024] It is used as a composite filter additive with an additive amount of 15 mg / cig. Taking the cigarette without adding any filter modified material as a control sample, the cigarette smoking test is carried out on a smoking machine according to the standard smoking conditions, and according to the standard YC / T255-2008 for the detection of phenol release. Three parallel samples were taken for each sample, and the results are shown in Table 1.

[0025] Table 1 R...

Embodiment 2

[0030] Prepare the oil phase first, the composition is 6ml styrene, 4ml divinylbenzene, 10ml xylene, 0.2g azobisisobutylcyanide, and then configure the water phase, the composition is 80 ml water, 0.5g calcium chloride and 2 g gelatin . Under stirring, the water phase was added into the oil phase, then the temperature was raised to 80° C., and the reaction was carried out for 12 hours. The obtained spherical product was extracted with ethanol for 24 hours to obtain the macroporous adsorption resin 2.

[0031] It is used as a composite filter additive with an additive amount of 15 mg / cig. Taking the cigarette without adding any filter modified material as a control sample, the cigarette smoking test is carried out on a smoking machine according to the standard smoking conditions, and according to the standard YC / T255-2008 for the detection of phenol release. Each sample has three parallel samples, and the results are shown in Table 2.

[0032] Table 2 Macroporous Adsorbent ...

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PUM

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Abstract

The invention relates to application of macroporous adsorption resin to cigarettes, which is characterized in that adding the macroporous adsorption resin to a filter of each cigarette can selectively reduce phenol release in mainstream smoke of the cigarette by more than 25%, 10-30mg of the macroporous adsorption resin is added per filter, and the macroporous adsorption resin obtained by suspension polymerization comprises divinyl benzene, styrene, pore-forming agent, initiator, water, inorganic salt and dispersant. The macroporous adsorption resin is capable of effectively adsorbing harmful phenol in smoke while tar release is substantially unchanged or slightly lowered, and has no adverse effect on smoking quality of the cigarettes, and accordingly the phenol release in the smoke of the cigarettes is selectively reduced.

Description

[0001] technical field [0002] The invention belongs to the field of additive materials for reducing harm of cigarettes, and in particular relates to the application of a macroporous adsorption resin which selectively reduces the amount of phenol released in mainstream smoke of cigarettes in reducing harm of cigarettes. Applying the material to cigarette filter rods can effectively reduce the amount of phenol released in mainstream smoke without negatively affecting the smoking quality of cigarettes. [0003] Background technique [0004] Phenol is one of the main harmful components of cigarette mainstream smoke. The volatile phenolic compounds in cigarette smoke are mainly produced during the burning process of cigarettes. According to the relationship between biological activity, phenol is one of the most important harmful components affecting the harmfulness of mainstream cigarette smoke. Therefore, reducing the phenol content in cigarette smoke is of great signif...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24D3/14
Inventor 杨松张晓兵孙学辉王宜鹏赵乐颜权平聂聪谢复炜刘惠民
Owner ZHENGZHOU TOBACCO RES INST OF CNTC
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