Universal refrigerant resistant solvent-free impregnating resin for high and low voltage motor and preparation method thereof
An impregnating resin, high and low voltage technology, which is applied in the field of general solvent-free impregnating resin for high and low voltage motors and its preparation, can solve the problems of non-environmental protection, large volatilization, inconvenient use, etc., and achieve the effect of low VOC content
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Embodiment 1
[0033] According to the formula of the solvent-free impregnation resin of the present embodiment is as follows:
[0034] 6kg of unsaturated polyesterimide resin solution with a solid content of 70%;
[0035] Solid content is 1.8kg of the polyoxazolidone resin solution of 80%;
[0036] Cross-linking monomer (vinyltoluene) 1.5kg;
[0037] Curing agent (chromium acetylacetonate) 0.35kg;
[0038] Initiator (dicumyl peroxide) 0.175kg;
[0039] Inhibitor (hydroquinone) 2.4g.
[0040] The preparation of described solvent-free impregnation resin comprises the steps:
[0041] (1), preparation solid content is the unsaturated polyesterimide resin solution of 70%: in a standard there-necked flask, add 252g neopentyl glycol, 116g isophthalic acid, 128g maleic anhydride, 53.4g pyrene Triformic anhydride (phenyl) imidic acid and 0.5g p-toluenesulfonic acid, heated up to 200°C under the protection of nitrogen, reacted for 5~6h, when the acid value dropped below 20mgKOH / g, cooled to 100°C,...
Embodiment 2
[0045] According to the formula of the solvent-free impregnation resin of the present embodiment is as follows:
[0046] 4.5kg of unsaturated polyesterimide resin solution with a solid content of 70%;
[0047] Solid content is 3.2kg of the polyoxazolidinone resin solution of 80%;
[0048] Cross-linking monomer (vinyltoluene) 2kg;
[0049] Curing agent (zirconium acetylacetonate) 0.5kg;
[0050] Initiator: 200g dicumyl peroxide + 40g tert-butyl peroxybenzoate;
[0051] Inhibitor (p-benzoquinone) 4.5g.
[0052] The preparation of described solvent-free impregnation resin comprises the steps:
[0053] (1), preparation solid content is the unsaturated polyesterimide resin solution of 70%: in a standard there-necked flask, add 238g neopentyl glycol, 26.1g Saike, 116g isophthalic acid, 14.6g adipic acid, 128g of maleic anhydride, 19.5g of tetrahydrophthalic anhydride iminoethyl alcohol and 0.45g of p-toluenesulfonic acid were heated to 200°C for 5-6 hours under the protection o...
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