Method for determining chrominum content in edible gelatine
A measurement method, the technology of edible gelatin, applied in the field of inspection and detection, can solve the problems of cumbersome and complicated operation, large consumption of reagents, poor accuracy, etc., and achieve the effect of reasonable detection method, fast analysis speed and wide linear range
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[0033] Embodiment one, the detection of 27 edible gelatin samples.
[0034]The 27 edible gelatin samples were all taken from edible gelatin sales stalls and enterprises, and the samples were tested separately. After being pulverized evenly, pass through a 800-mesh sieve, weigh 2.5 g and place it in a polytetrafluoroethylene tank, add 4 mL of nitric acid and soak for 24 hours. Then add 2 mL of 30% hydrogen peroxide, cover the inner cover, tighten the stainless steel jacket, put it into the microwave digestion instrument, and set the parameters of the microwave digestion instrument for digestion. Digestion includes four stages: the first stage set the pressure 0.5MPa, power 600W, run for 5 minutes; the second stage set the pressure 1.0MPa, power 600W, run for 3 minutes; the third stage set the pressure 1.5MPa, power 600W, run for 3 minutes ; In the fourth stage, set the pressure to 1.8MPa, power to 800W, and run for 5 minutes. After digestion, cool to room temperature, filter ...
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