Method for detecting quality of tobacco flavor
A technology of tobacco flavor and detection method, which is applied in the directions of measuring devices, instruments, scientific instruments, etc., can solve the problems of low accuracy of results and limited application, etc.
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[0104] Use a pipette gun to pipette 400 μL of tobacco flavor samples D, E, F, G, J, K, L and N into 4 mL sample bottles, add 800 μL of dichloromethane to it, shake well and place on a rotary shaker Shake it up for 10 minutes, let it stand for 10 minutes, remove the lower organic layer, then add 1 g of anhydrous sodium sulfate to the obtained lower organic layer, dry it at room temperature for 30 minutes, and perform GC / MS analysis.
[0105] GC / MS analysis conditions are:
[0106] Chromatographic column: HP-5MS (60m×0.25mm×0.25μm) quartz capillary column; carrier gas: He; flow rate: 1mL / min; inlet temperature: 280°C; split ratio: 10:1; injection volume: 1 μL; temperature program:
[0107] Interface temperature: 280°C; ion source: EI; ionization energy: 70eV; ion source temperature: 230°C; quadrupole temperature: 150°C; solvent delay: 6min; scan range: 40~350amu.
[0108] The results of chromatographic analysis were as figure 1 as shown, figure 1 For the chromatographic an...
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