ZrC (Zirconium Carbide) ceramic precursor, ZrC ceramic and preparation method thereof
A ceramic precursor and ceramic technology, applied in the field of ceramics, can solve the problems of low yield of ZrC ceramics, inability to store for a long time, poor operability, etc., and achieve the effects of fine grains, complete mutual dissolution and good crystallinity
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[0037] Another aspect of the present invention also provides a method for preparing the aforementioned ZrC ceramic, including the following steps:
[0038] 1. Cross-linking the aforementioned ZrC ceramic precursor solution at a cross-linking reaction temperature of 100-250°C for 0.5-4 hours to obtain a cross-linked ZrC ceramic precursor;
[0039] 2. The cross-linked ZrC ceramic precursor is subjected to a cracking reaction at a cracking reaction temperature of 1400 to 1600°C for 0.5 to 2 hours under an inert atmosphere or a vacuum condition to obtain ZrC ceramics.
[0040] The preparation method of ZrC ceramic provided by the present invention, because the zirconium source and the bidentate ligand form a coordinated intermediate, the mutual dissolution with the carbon source is more thorough, the combination is tighter, and the energy loss during the combination process between the carbon source and the zirconium source is reduced , The cracking reaction temperature is lower, and the...
Example Embodiment
[0045] Example 1
[0046] a) ZrOCl with a molar ratio of 1:1:2:9 2 ·8H 2 O, phenolic resin, acetylacetone and absolute ethanol are placed in a container and stirred evenly to obtain a ZrC ceramic precursor;
[0047] b) Keep the ZrC ceramic precursor at 100°C for 2 hours to obtain a cross-linked precursor gel;
[0048] c) Put the precursor gel into the mold, put it into the high-temperature cracking furnace, heat it up to 1400°C and keep it for 2 hours, then take it out to obtain the ZrC ceramic.
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[0049] Example 2
[0050] a) ZrOCl with a molar ratio of 1:3:1:2 2 ·8H 2 O. Phenolic resin, ethylene glycol and absolute ethanol are placed in the container and stirred evenly to obtain the ZrC ceramic precursor;
[0051] b) Keep the ZrC ceramic precursor at 250°C for 0.5 hours to obtain a crosslinked precursor gel;
[0052] c) Put the precursor gel into a mold, put it into a high-temperature cracking furnace, heat it up to 1600°C, keep it for 0.5 hours, and take it out to obtain ZrC ceramics.
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