Multiple-effect type semi-synthetic micro-emulsion cutting solution
A semi-synthetic and micro-emulsion technology, applied in lubricating compositions, petroleum industry, additives, etc., can solve the problems of large environmental pollution and poor biodegradability, and achieve good biological stability, good environmental protection, excellent corrosion inhibition and anti-corrosion. The effect of rust properties
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Embodiment 1
[0043] First prepare the phosphorus-containing borate water-based lubricant:
[0044] (1) Put boric acid, raw material A, and glycerol into the reaction kettle, and conduct the reaction under vacuum and constant stirring. The reaction temperature is 80°C and the reaction time is 120 minutes;
[0045] (2) Turn off the vacuum, cool the temperature in the reactor to below 50℃, then slowly add phosphorus pentoxide to the reactor, keep stirring, control the reaction temperature below 90℃, and stir for 1 hour after the addition is complete;
[0046] (3) Control the temperature below 90℃, add pure water to the reactor and stir for 60 minutes;
[0047] (4) The temperature of the reactor is lowered to room temperature, and the material is discharged to obtain a phosphorus-containing borate water-based lubricant.
[0048] Then mix tap water, monoethanolamine, benzotriazole, boric acid, No. 5 white oil, base oil 150SN, tall oil fatty acid, sebacic acid, borophosphate water-based lubricant, propyle...
Embodiment 2
[0050] First prepare the phosphorus-containing borate water-based lubricant:
[0051] (1) Put boric acid, raw material A, and glycerol into the reaction kettle, and conduct the reaction under vacuum and continuous stirring. The reaction temperature is 120°C and the reaction time is 60 minutes;
[0052] (2) Turn off the vacuum, cool the temperature in the reactor to below 50℃, then slowly add phosphorus pentoxide to the reactor, keep stirring, control the reaction temperature below 90℃, and stir for 50 minutes after the addition is complete;
[0053] (3) Control the temperature below 90℃, add pure water to the reactor and stir for 70 minutes;
[0054] (4) The temperature of the reactor is lowered to room temperature, and the material is discharged to obtain a phosphorus-containing borate water-based lubricant.
[0055] Then mix tap water, monoethanolamine, benzotriazole, boric acid, No. 5 white oil, base oil 150SN, tall oil fatty acid, sebacic acid, borophosphate water-based lubricant, p...
Embodiment 3
[0057] First prepare the phosphorus-containing borate water-based lubricant:
[0058] (1) Put boric acid, raw material A, and glycerol into the reaction kettle, and conduct the reaction under vacuum and constant stirring conditions, the reaction temperature is 100°C, and the reaction time is 100 minutes;
[0059] (2) Turn off the vacuum, cool the temperature in the reactor to below 50℃, then slowly add phosphorus pentoxide to the reactor, keep stirring, control the reaction temperature below 90℃, and stir for 70 minutes after the addition is complete;
[0060] (3) Control the temperature below 90℃, add pure water to the reactor and stir for 80 minutes;
[0061] (4) The temperature of the reactor is lowered to room temperature, and the material is discharged to obtain a phosphorus-containing borate water-based lubricant.
[0062] Then mix tap water, monoethanolamine, benzotriazole, boric acid, No. 5 white oil, base oil 150SN, tall oil fatty acid, sebacic acid, borophosphate water-based l...
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