Electric conduction dust-free health care carbon granule

A carbon particle, microwave treatment technology, applied in the polymer field, can solve the problems of health care function to be improved, poor stability, poor antistatic property, etc. Effect

Active Publication Date: 2014-08-13
烟台力量知识产权服务有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005]The above-mentioned methods all carbonize block wood or bamboo, and all of them are heated up to the sintering temperature and immediately cooled down, so there are uneven carbonization, poor stability, and poor electrical conductivity. Low, poor antistatic properties, etc.
And it contains dust and impurities, and the health care function needs to be improved

Method used

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  • Electric conduction dust-free health care carbon granule
  • Electric conduction dust-free health care carbon granule

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] The plant raw material used in this embodiment is corncob.

[0036] Put the plant material into the microwave vacuum tank, vacuumize to -0.02MPa, and then conduct microwave treatment, the microwave frequency is 300MHz, and the microwave treatment time is 1min; the plant material obtained after pretreatment is dried and pre-carbonized in sequence , carbonization, calcination and cooling, the temperature of each temperature measurement point, the drying zone A is 150°C, the pre-carbonization zone B is 275°C, and the carbonization zone C is 450°C. figure 1 The zone D shown is the temperature of different positions in the combustion zone. When the temperature of a certain place in the combustion zone, such as d2, is too low, open the small hole in that place, introduce air and burn it nearby, so as to raise the temperature in this place and control the bamboo to move down. The temperature of the combustion zone experienced during the process, control the combustion to rais...

Embodiment 2

[0041] The plant material used in this example is bamboo chips (about 40 cm long).

[0042] Put the plant material into the microwave vacuum tank, vacuumize until the vacuum degree is -0.001MPa, and then carry out microwave treatment, the microwave frequency is 950MHz, and the microwave treatment time is 3min;

[0043] The plant raw materials obtained through pretreatment are dried, pre-carbonized, carbonized, calcined, and cooled in sequence. The temperature at each temperature measurement point is 150°C in drying area A, 275°C in pre-carbonization area B, and 450°C in carbonization area C. Observation during warming figure 1 The zone D shown is the temperature of different positions in the combustion zone. When the temperature of a certain place in the combustion zone, such as d2, is too low, open the small hole in that place, introduce air and burn it nearby, so as to raise the temperature in this place and control the bamboo to move down. The temperature of the combustio...

Embodiment 3

[0047] The plant raw material used in this embodiment is pine tree, and the pine tree is first cut after the skin impurities are removed, and the length is controlled to be no more than 15 cm.

[0048] Put the plant raw material into the microwave vacuum tank, evacuate until the vacuum degree is -0.01~-0.005MPa, and then carry out microwave treatment, the microwave frequency is 550MHz, and the microwave treatment time is 1.2-2min;

[0049] The pre-treated plant raw materials are dried, pre-carbonized, carbonized, calcined, and cooled in sequence. The temperature at each temperature measurement point is 180°C in the drying area A, 325°C in the pre-carbonization area B, and 530°C in the carbonization area C. Observation during warming figure 1 The zone D shown is the temperature of different positions in the combustion zone. When the temperature of a certain place in the combustion zone, such as d2, is too low, open the small hole in that place, introduce air and burn it nearby...

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Abstract

The invention relates to the field of polymers, in particular to a conductive dust-free health-care carbon particle. It is made through the following steps: Raw material pretreatment: put the plant raw material into a microwave vacuum tank, vacuumize it, and then carry out microwave treatment; then undergo drying, pre-carbonization, carbonization, calcination and cooling in sequence, and control the combustion at 5-15°C Raise the temperature to 700-750°C or 900-1000°C at a rate of 5-15°C / min and keep it warm for 40-80 minutes, then raise the temperature to 1000-1500°C or 1600-1800°C at a rate of 5-15°C / min and keep it warm for 2-8 hours, then Cool down to 300-400°C at a rate of 18-25°C / min, and then cool to room temperature with the furnace to obtain primary carbon; soaking treatment: soak the obtained primary carbon in a solution with an acid content of 3-5wt% for 20-40min , and then mixed and submerged with potassium oxalate solution with a mass fraction of 8-10% according to a mass ratio of 1:3-4 for 3-5h, and then washed with deionized water until the pH value is neutral; microwave treatment; carbon particle preparation. The carbon particles prepared by the invention do not contain dust and impurities, have good antistatic properties, and have health care functions.

Description

technical field [0001] The invention relates to the field of polymers, in particular to a conductive dust-free health-care carbon particle. Background technique [0002] At present, the methods for firing wood charcoal materials include a one-time carbonization firing method and a graded temperature-controlled firing method. [0003] The secondary carbonization firing method is a method in which the incompletely carbonized wood charcoal is sintered at a high temperature to prepare a conductive wood charcoal material. For example, Japanese patent JP 2005035806 conductive charcoal or bamboo charcoal and its preparation method is a method for preparing conductive charcoal or bamboo charcoal by carbonizing block charcoal or bamboo charcoal at a temperature above 1000°C once. The carbon yield of this preparation method is high, but the sintering process requires a second temperature rise for sintering, and the carbon oxidation is likely to occur during the second sintering proce...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B31/02C01B32/05
Inventor 丁建中
Owner 烟台力量知识产权服务有限公司
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