AnodePositive electrode material of lithium ion battery with porous laminated structure and preparation method thereof
A technology for lithium-ion batteries and positive electrode materials, applied in battery electrodes, structural parts, circuits, etc., can solve the problems of increased side reactions, decreased cycle stability, and failure to reach, and achieve improved contact, simplified preparation process, and long-term use. The effect of longevity
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[0030] Example 1
[0031] 1) Dissolve 1.5g agar powder (agar powder, purified (RB), Sinopharm Chemical Reagent Co., Ltd.) in 100 mL deionized water, stir at 95°C to dissolve it to form a transparent hot agar solution. According to the molar ratio of 1.236:0.54:0.13:0.13, the raw material LiNO 3 , Mn(CH 3 COO) 2 ·4H 2 O, Ni(NO 3 ) 2 ·6H 2 O and Co(NO 3 ) 2 ·6H 2 O is dissolved in the hot agar solution (3% excess lithium salt is added to offset the loss of lithium at high temperature) to form a red transparent solution. The red transparent solution contains lithium, nickel, manganese and cobalt salts The total concentration is 0.5mol / L. The obtained red transparent solution was cooled to 20°C to obtain a red jelly-like gel. Put the red jelly-like gel in a riot freezer and freeze to -20°C, and put the frozen cryogel in a freeze dryer at -60°C for 3 days to remove moisture from it to obtain an aerogel.
[0032] 2) Put the aerogel in a box furnace, heat it up to 500°C at a heating rat...
Example Embodiment
[0037] Example 2
[0038] 1) Dissolve 1.5g agar powder (agar powder, purified (RB), Sinopharm Chemical Reagent Co., Ltd.) in 100 mL deionized water, stir at 95°C to dissolve it to form a transparent hot agar solution. According to the molar ratio of 1.236:0.54:0.13:0.13, the raw material LiNO 3 , Mn(CH 3 COO) 2 ·4H 2 O, Ni(NO 3 ) 2 ·6H 2 O and Co(NO 3 ) 2 ·6H 2 O is dissolved in the hot agar solution (3% excess lithium salt is added to offset the loss of lithium at high temperature) to form a red transparent solution. The red transparent solution contains lithium, nickel, manganese and cobalt salts The total concentration is 0.5mol / L. The obtained red transparent solution was cooled to 30°C to obtain a red jelly-like gel. Put the red jelly-like gel in a riot freezer and freeze to -20°C, and put the frozen cryogel in a freeze dryer at -50°C for 2 days to remove moisture from it to obtain an aerogel.
[0039] 2) Put the aerogel in a box furnace, heat it up to 550°C at a temperature...
Example Embodiment
[0044] Example 3
[0045] Dissolve 1.5g agar powder (agar powder, purified (RB), Sinopharm Chemical Reagent Co., Ltd.) in 100 mL deionized water, stir at 90°C to dissolve it to form a transparent hot agar solution. According to the molar ratio of 1.236:0.56:0.16:0.08, the raw material LiNO 3 , Mn(CH 3 COO) 2 ·4H 2 O, Ni(NO 3 ) 2 ·6H 2 O and Co(NO 3 ) 2 ·6H 2 O is dissolved in the hot agar solution (3% excess lithium salt is added to offset the loss of lithium at high temperature) to form a red transparent solution. The red transparent solution contains lithium, nickel, manganese and cobalt salts. The total concentration is 0.2mol / L. The obtained red transparent solution was cooled to 25°C to obtain a red jelly-like gel. Put the red jelly-like gel in a riot freezer and freeze to -20°C, and put the frozen cryogel in a freeze dryer at -60°C for 3 days to remove moisture from it to obtain an aerogel. Put the aerogel in a box furnace, heat it up to 450°C at a rate of 10°C / min in an ...
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