Light Al2O3-SiC-C refractory brick and preparation method thereof

A technology of al2o3-sic-c and refractory bricks, which is applied in the field of lightweight refractory bricks, can solve the problems of not using lightweight refractory materials, and achieve excellent thermal shock stability, excellent thermal shock stability, and strong resistance to medium erosion Effect

Inactive Publication Date: 2013-03-20
WUHAN UNIV OF SCI & TECH
View PDF3 Cites 22 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the research on lightweight refractory materials mainly focuses on the heat insulation refractory materials used in the insulation layer of high-temperature kilns, while there are few studies on lightweight refractory materials

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A light Al 2 o 3 -SiC-C refractory brick and its preparation method: 15~18wt% of porous corundum particles with a particle size of 5~3mm, 30~35wt% of porous corundum particles with a particle size of 3~1mm, 10~12wt% of porous corundum particles Porous corundum particles with a diameter of less than 1mm, 18~22% white corundum fine powder, 4~6wt% SiC particles, 4~6wt% SiC fine powder, 6~9wt% flake graphite, 1.5~2.5wt% Silicon powder and 0.2~0.6wt% aluminum powder are used as raw materials, and 3.5~5wt% liquid phenolic resin is added to the raw materials, stirred evenly, and machine-pressed; then the molded green body is processed at 220~240°C for 12 ~24 hours, then keep it warm at 1400~1450℃ and reducing atmosphere for 2~6 hours.

[0028] In this embodiment: the apparent porosity of the porous corundum particles is 25-35%, and the average pore diameter is 10-20 μm.

[0029] Adopting the technical scheme described in this embodiment, the obtained apparent porosity is 28...

Embodiment 2

[0031] A light Al 2 o 3 -SiC-C refractory brick and its preparation method: 12~15wt% of porous corundum particles with a particle size of 5~3mm, 25~30wt% of porous corundum particles with a particle size of 3~1mm, 8~10wt% of porous corundum particles Porous corundum particles with diameter less than 1mm, 22~25% tabular corundum fine powder, 6~8wt% SiC particles, 6~8wt% SiC fine powder, 9~12wt% flake graphite, 1.5~2.5wt% Silicon powder and 0.2~0.6wt% aluminum powder are used as raw materials, plus 3.5~5wt% solid phenolic resin powder of the raw materials, stirred evenly, and machine-pressed; Treat for 24~36 hours, then keep it warm at 1450~1500℃ and reducing atmosphere for 2~6 hours.

[0032] In this embodiment: the apparent porosity of the porous corundum particles is 32-40%, and the average pore diameter is 1-10 μm.

[0033] Adopting the technical scheme described in this embodiment, the obtained apparent porosity is 34~41%, and the bulk density is 2.16~2.43g / cm 3 and lig...

Embodiment 3

[0035] A light Al 2 o 3-SiC-C refractory brick and its preparation method: 12~18wt% of porous corundum particles with a particle size of 5~3mm, 28~32wt% of porous corundum particles with a particle size of 3~1mm, 9~11wt% of porous corundum particles Porous corundum particles with diameter less than 1mm, 10~12wt% white corundum fine powder, 10~12wt% platy corundum fine powder, 5~7wt% SiC particles, 5~7wt% SiC fine powder, 8~10wt% % flake graphite, 1.5~2.5wt% silicon powder and 0.2~0.6wt% aluminum powder as raw materials, plus 3.5~5wt% liquid phenolic resin of the raw materials, stir evenly, and machine press molding; then the molded The green body is treated at 210-230°C for 12-24 hours, and then kept at 1420-1470°C and reducing atmosphere for 2-6 hours.

[0036] In this embodiment: the apparent porosity of the porous corundum particles is 30-38%, and the average pore diameter is 5-15 μm.

[0037] Adopting the technical scheme described in this embodiment, the obtained appar...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Particle sizeaaaaaaaaaa
Particle sizeaaaaaaaaaa
Particle sizeaaaaaaaaaa
Login to view more

Abstract

The invention relates to a light Al2O3-SiC-C refractory brick and a preparation method thereof. The preparation method comprises the steps of: taking 45-65wt% of porous corundum particles, 18-25% of fine corundum powder, 4-8wt% of SiC particles, 4-8wt% of fine SiC powder, 6-12wt% of crystalline flake graphite, 1.5-2.5wt% of ganister sand and 0.2-0.6wt% of aluminite powder as materials; adding 3.5-5wt% of phenolic resin to evenly stir; and mechanically pressing and molding, carrying out heat preservation on the molded billet for 12-36 hours at 200-240 DEG C, and then carrying out heat preservation for 2-6 hours at 1400-1500 DEG C under the condition of reducing atmosphere, so as to obtain the light Al2O3-SiC-C refractory brick. The light Al2O3-SiC-C refractory brick is simple in preparation process; the prepared light Al2O3-SiC-C refractory brick not only has the characteristics of high strength, excellent thermal shock resistance, strong medium erosion resistance and low thermal conductivity, but also has the characteristics of apparent porosity and pore size controllability, and is suitable for the devices such as torpedo hot metal mixer cars, metal mixers, and ladles (tanks).

Description

technical field [0001] The invention belongs to the technical field of lightweight refractory bricks. Specifically related to a light Al 2 o 3 -SiC-C refractory brick and its preparation method. Background technique [0002] Refractory materials are composed of aggregate and matrix, and the matrix is ​​relatively loose. During the use of refractory materials, solvents such as slag first corrode the matrix. The matrix surrounds the aggregate, and when the matrix is ​​eroded into a metamorphic layer, the aggregate is spalled with the matrix from the refractory into the slag. Therefore, in terms of corrosion resistance, the effect of dense aggregate is not obvious. Al is used in the preparation of traditional torpedo-type mixed iron cars, mixed iron furnaces and ladles (cans) 2 o 3 -SiC-C and Al 2 o 3 -SiC refractories, people often use dense materials as aggregates, such as white corundum, brown corundum or alumina. In order to prepare dense aggregate, raw materials ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C04B38/08C04B35/66C04B35/622
Inventor 鄢文李楠苗正陈俊峰魏耀武韩兵强柯昌明
Owner WUHAN UNIV OF SCI & TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products