Environment-friendly indium oxide hydro-thermal synthesis method
An environmentally friendly, hydrothermal synthesis technology, applied in chemical instruments and methods, gallium/indium/thallium compounds, inorganic chemistry, etc., can solve the problems of surfactant loss, product loss, high cost, and reduce surfactants. churn, product loss reduction, emission reduction effect
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Embodiment 1
[0021] (1). Preparation of precursor indium hydroxide
[0022] a. Under magnetic stirring conditions, in 70.00ml deionized water, add 0.5006g surfactant and 0.8006g InCl 3 4H 2 O, keep stirring to make it evenly dispersed, add 0.5000g solid NaOH, stir to dissolve it, obtain a uniform solution, continue to stir for 25 minutes,
[0023] b. Then move to a polytetrafluoroethylene container, seal it in a stainless steel autoclave, heat and react at 220°C for 20 hours, then cool to room temperature,
[0024] c. The product is separated by centrifugation and washed, and the precipitate is dried and ground to obtain indium hydroxide In(OH) 3 ;
[0025] (2). Preparation of environmentally friendly indium oxide
[0026] Indium hydroxide In(OH) obtained by drying and grinding 3 Calcined at 500°C for 2 hours to obtain cubic indium oxide;
[0027] The filtrate after the centrifugation in the step (1) enters the filtrate storage tank, the sample after the centrifugation is washed t...
Embodiment 2
[0029] (1). Preparation of precursor indium hydroxide
[0030] a. Under magnetic stirring conditions, in 80.00ml deionized water, add 0.8004g surfactant and 0.9008g InCl 3 4H 2 O, keep stirring to make it uniformly dispersed, add 0.8000g solid NaOH and stir to dissolve it, obtain a uniform solution, continue to stir for 30 minutes,
[0031] b. Then move to a polytetrafluoroethylene container, seal it in a stainless steel autoclave, heat and react at 230°C for 18 hours, then cool to room temperature,
[0032] c. The product is separated by centrifugation and washed, and the precipitate is dried and ground to obtain indium hydroxide In(OH) 3 ;
[0033] (2). Preparation of environmentally friendly indium oxide
[0034] Indium hydroxide In(OH) obtained by drying and grinding 3 Calcined at 550°C for 1.5 hours to obtain cubic indium oxide;
[0035] The filtrate after the centrifugation in the step (1) enters the filtrate storage tank, the sample after the centrifugation is ...
Embodiment 3
[0037] (1). Preparation of precursor indium hydroxide
[0038] a. Under the condition of magnetic stirring, in 85.00ml deionized water, add 1.0054g surfactant and 1.0001gInCl 3 4H 2 O, keep stirring to make it evenly dispersed, add 1.0000g of solid NaOH, stir to make it dissolve, obtain a uniform solution, continue to stir for 35 minutes,
[0039] b. Then move to a polytetrafluoroethylene container, seal it in a stainless steel autoclave, heat and react at 250°C for 16 hours, then cool to room temperature,
[0040] c. The product is separated by centrifugation and washed, and the precipitate is dried and ground to obtain indium hydroxide In(OH) 3 ;
[0041] (2). Preparation of environmentally friendly indium oxide
[0042] Indium hydroxide In(OH) obtained by drying and grinding 3 Calcined at 600°C for 1 hour to obtain cubic indium oxide;
[0043]The filtrate after the centrifugation in the step (1) enters the filtrate storage tank, the sample after the centrifugation ...
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