Method for preparing aromatic polyamide fiber paper base material by electrospinning technology
An electrospinning technology and aramid fiber technology are applied in the field of preparing aramid fiber paper-based materials by using electrospinning technology, which can solve the problems of low forming strength, difficulty in guaranteeing hot-pressing performance, and restricting the development of large-scale development. Good mechanical properties and heat resistance, simple process and high efficiency
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0022] 1. Take 53ml of dimethylacetamide (DMAc) and 2g of anhydrous lithium chloride in an Erlenmeyer flask, seal it and place it in an oil bath, stir at 80℃ for about 20 minutes and then dissolve the lithium chloride, add accurately Good 2.5g aramid fiber pulp, after sealing, stir for 2h at 80℃, the pulp will swell and dissolve to form a uniform translucent light yellow solution. After taking it out, let it stand for 30min at room temperature, fully swell and dissolve to remove bubbles. Uniform and transparent 5% aramid fiber solution.
[0023] 2. Electrospin the prepared aramid fiber solution under high pressure. The electrospinning conditions are: voltage 18kv, spinning dope advancing speed 0.1ml / h, temperature 30℃, relative humidity 20%, rotation speed 4.8 r / min, the receiving distance is 8cm, and the receiving device of the electrostatic spinning device is a flat plate collection.
[0024] 3. The aramid fiber membrane was immersed in deionized water for 2 hours and dried at 8...
Embodiment 2
[0026] 1. Take 53ml of dimethylacetamide (DMAc) and 3.5g of anhydrous lithium chloride in an Erlenmeyer flask, seal it and place it in an oil bath, stir at 80℃ for about 20 minutes and then dissolve the lithium chloride. Add it accurately Weighed 5g aramid fiber pulp, sealed and stirred at 80℃ for 2h, the pulp swelled and dissolved to form a uniform translucent light yellow solution. After taking it out, let it stand at room temperature for 45 minutes, fully swelled and dissolved to remove bubbles. Uniform and transparent 10% aramid fiber solution.
[0027] 2. Electrospin the prepared aramid fiber solution under high pressure. The electrospinning conditions are: voltage 24kv, spinning solution advancing speed 0.7ml / h, temperature 35℃, relative humidity 25%, speed 5.2 r / min, the receiving distance is 10cm, and the receiving device of the electrostatic spinning device is roller collection.
[0028] 3. The aramid fiber membrane was immersed in deionized water for 2 hours and dried at...
Embodiment 3
[0030] 1. Take 53ml of dimethylacetamide (DMAc) and 5g of anhydrous lithium chloride in an Erlenmeyer flask, seal it and place it in an oil bath, stir at 80°C for about 20 minutes and then dissolve the lithium chloride, add accurately Good 7.5g aramid fiber pulp, sealed and stirred at 80℃ for 2h, the pulp swells and dissolves to form a uniform translucent light yellow solution. After taking it out, let it stand for 60min at room temperature, fully swelling and dissolving to remove air bubbles. Uniform transparent 15% aramid fiber solution.
[0031] 2. Electrospin the prepared aramid fiber solution under high pressure. The electrospinning conditions are: voltage 30kv, spinning solution advancing speed 1.2ml / h, temperature 40℃, relative humidity 30%, rotation speed 6.2 r / min, the receiving distance is 12cm, and the receiving device of the electrostatic spinning device is roller collection.
[0032] 3. The aramid fiber membrane was immersed in deionized water for 2 hours and dried at...
PUM
Property | Measurement | Unit |
---|---|---|
thickness | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com