Umbrella-shaped electrostatic spinning sprayer and electrostatic spinning method

An electrospinning, umbrella-shaped technology, applied in the field of umbrella-shaped electrospinning nozzles and electrospinning, can solve problems such as affecting production efficiency, increasing conveying speed, and being difficult to maintain, achieving continuous and large-scale production, and easy to solve problems. The effect of blocking and improving production efficiency

Active Publication Date: 2013-05-08
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is serious mutual interference in the electric field between needle-type spinneret holes, and it is difficult to obtain large-scale promotion
Moreover, in the traditional electrospinning process, the propulsion speed of the infusion is slow, and the flow rate of the spinning solution is small. The method of increasing the delivery speed cannot guarantee the stability of the spinning and cannot carry out normal production.
In addition, affected by the viscosity and spinnability of the spinning solution, the diameter of the spinneret hole is mostly in the micron level, which is prone to clogging due to too fast volatilization of the solvent, resulting in production interruption, which affects production efficiency, and is difficult to maintain and difficult to clean. defect
At present, the open-up spinneret studied by some scholars has improved the needle spinneret to a certain extent, but there are still many shortcomings, such as the surface viscosity of the polymer solution caused by solvent volatilization, and it is difficult to form a stable jet under the same parameter conditions. , or the instability of the jet will affect the smooth progress of the spinning process, or the increase in the number of jets is limited, and the increase in the output of nanofibers is not obvious, etc.

Method used

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  • Umbrella-shaped electrostatic spinning sprayer and electrostatic spinning method
  • Umbrella-shaped electrostatic spinning sprayer and electrostatic spinning method
  • Umbrella-shaped electrostatic spinning sprayer and electrostatic spinning method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] use figure 1 The new umbrella-shaped electrospinning nozzle shown is used for spinning. The solution is polyvinyl alcohol (PVA) aqueous solution with a mass concentration of 10%. The output end 2 of the solution propeller of the numerically controlled infusion device is placed in the middle of the umbrella-shaped spinneret 1. In the cylindrical hollow 8, the spinning solution will emerge from the top layer of the umbrella-shaped spinneret 1, forming a spinning solution layer with a uniform thickness and a certain curvature in all directions of each layer of copper plate. The distance between the receiving base fabric and the upper end of the umbrella-shaped spinneret 1 is kept at 20cm, the controller 3 is turned on, the voltage of the high-voltage generator is adjusted to 50kV, the base fabric moves at a speed of 0.01m / min, and the trolley carrying the spinneret does reciprocating motion. The diameters of the manufactured nanofibers are mostly distributed between 200~...

Embodiment 2

[0031] An umbrella-shaped electrospinning nozzle, including an umbrella-shaped spinneret 1, a numerically controlled infusion device and a solution collection tank 4, characterized in that the numerically controlled infusion device mainly includes a solution propeller 2 and a controller 3 There is a cylindrical hollow place 8 in the middle part of the umbrella spinneret 1, and the output end of the solution propeller 2 is inserted into the cylindrical hollow place 8 of the umbrella spinneret 1; the control Device 3 controls the flow rate and the flow rate of spinning solution, and continuously injects spinning solution into the top layer of the umbrella-shaped spinneret 1; the bottom of the umbrella-shaped spinneret 1 is placed with the solution collection tank 4; The spinneret 1 is provided with a terminal 6 connected with the high voltage positive electrode 5 . The axis of the described cylindrical hollow place 8 coincides with the central axis of the described umbrella spin...

Embodiment 3

[0033] An umbrella-shaped electrospinning nozzle, including an umbrella-shaped spinneret 1, a numerically controlled infusion device and a solution collection tank 4, characterized in that the numerically controlled infusion device mainly includes a solution propeller 2 and a controller 3 There is a cylindrical hollow place 8 in the middle part of the umbrella spinneret 1, and the output end of the solution propeller 2 is inserted into the cylindrical hollow place 8 of the umbrella spinneret 1; the control Device 3 controls the flow rate and the flow rate of spinning solution, and continuously injects spinning solution into the top layer of the umbrella-shaped spinneret 1; the bottom of the umbrella-shaped spinneret 1 is placed with the solution collection tank 4; The spinneret 1 is provided with a terminal 6 connected with the high voltage positive electrode 5 . The axis of the cylindrical hollow 8 coincides with the central axis of the umbrella spinneret 1 .

[0034] The el...

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PUM

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Abstract

The invention relates to an umbrella-shaped electrostatic spinning sprayer and an electrostatic spinning method. The sprayer comprises an umbrella-shaped spinning nozzle, a numerical control type infusion device and a solution collecting groove, wherein the numerical control type infusion device mainly comprises a solution propeller and a controller; the middle of the umbrella-shaped spinning nozzle is provided with a cylindrical hollow portion, and an output end of the solution propeller is placed into the cylindrical hollow portion of the umbrella-shaped spinning nozzle; the controller controls flow velocity and flow of spinning solutions; and the solution collecting groove is placed in the bottom of the umbrella-shaped spinning nozzle. The electrostatic spinning method comprises that a binding post on the umbrella-shaped spinning nozzle is connected with a high-voltage positive electrode, conducting polymer solutions are continuously added to the umbrella-shaped spinning nozzle which is horizontally placed through the numerical control type infusion device, electrostatic spinning is started, collection is achieved through a collecting device, and nano-fibers are formed. The sprayer avoids blocking phenomena, and is easy to clean and good in stability; and the electrostatic spinning method improves production efficiency and the yield of electrostatic spinning.

Description

technical field [0001] The invention belongs to the field of electrostatic spinning devices and methods thereof, in particular to an umbrella-shaped electrostatic spinning nozzle and an electrostatic spinning method. Background technique [0002] Electrospinning is a relatively popular simple method for manufacturing nanofibers. It has become a hot spot in the current research on nanofiber manufacturing due to its excellent characteristics such as simple equipment, easy operation, wide source of materials, and no damage to the material body during the process. The nanofibers produced by electrospinning have the characteristics of small diameter, large specific surface area, and high porosity, and have great application potential in the fields of biomedicine, air filtration, and protective clothing. [0003] Electrospinning is to bring the polymer solution to thousands or even tens of thousands of volts of high-voltage static electricity. The charged droplets form a Taylor co...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01D5/00D01D4/02
Inventor 覃小红蒋国军王衍书
Owner DONGHUA UNIV
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