Optical adhesive, optical adhesive and display apparatus comprising the same
A technology of optical adhesives and optical components, applied in the direction of optical components, adhesive types, ester copolymer adhesives, etc., can solve the problems of degraded display device usability, ITO film corrosion, etc.
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preparation example 1
[0080] Preparation Example 1: Preparation of (meth)acrylic acid copolymer
[0081] 59 parts by weight of butyl acrylate (BA), 10 parts by weight of methyl acrylate (MA), 0.5 parts by weight of 2-hydroxyethyl acrylate (2-HEMA), 30 parts by weight of phenoxymethacrylate (PMA ) and 0.5 parts by weight of acrylic acid (AA) and 10 parts by weight of ethyl acetate (EA) as a solvent were put together in a 1 L 4-necked flask and kept at 65°C. 0.03 parts by weight of azobisisobutyronitrile diluted with ethyl acetate in a ratio of 50% was added to the mixture as an initiator. A (meth)acrylic copolymer was prepared by reacting at 65°C for 5 hours. During the reaction, nitrogen gas was supplied into the flask at 10 cc / min. The refractive index of the prepared (meth)acrylic copolymer can be measured by a typical method of measuring the refractive index of a film with an Abbe refractometer. The acid value of the prepared (meth)acrylic copolymer was measured according to JIS K0070 (1992 e...
preparation example 2 to 5
[0082] Preparation Examples 2 to 5: Preparation of (meth)acrylic acid copolymer
[0083] A (meth)acrylic copolymer was prepared in the same manner as in Preparation Example 1 except for the contents of individual components (unit: parts by weight).
[0084] Table 1
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[0086]
[0087] Details of the components used in Examples and Comparative Examples are as follows.
[0088] (1) (meth)acrylic acid copolymer: (meth)acrylic acid copolymer prepared by embodiment 1 to 5
[0089] (2) Curing agent 1: Trimethylolpropane modified toluene diisocyanate (Coronate-L, Nippon Polyurethane)
[0090] Curing agent 2: epoxy resin crosslinking agent (TETRAD-C, Mitsubishigano)
[0091] (3) Silane coupling agent: 3-glycidyloxypropyltrimethoxysilane (KBM-403, Shin-Etsu Chemical)
Embodiment 1 to 3 and comparative example 1 to 2
[0092] Examples 1 to 3 and Comparative Examples 1 to 2: Preparation of Optical Adhesives
[0093] Each optical adhesive was prepared by mixing the components (unit: parts by weight) listed in Table 2 excluding the solvent, and then stirring the mixture for 1 hour.
[0094] Table 2
[0095]
[0096] The properties of each prepared optical adhesive were evaluated as follows, and the results are shown in Table 3.
[0097] (1) Corrosion property: The prepared adhesive is coated on a polarizing plate to a thickness of 20 to 30 μm. Then, the coated adhesive layer was cured at 35°C for 5 days, and two ITO films were stacked on the opposite upper side of the cured adhesive layer, thereby providing figure 2 Samples shown. The sample of the cured adhesive layer stacked on the polarizing plate has a total length Y of 7 cm, each of the ITO films stacked on the opposite upper side of the cured adhesive layer has a length X of 1 cm, and for surface resistance The measured length Z i...
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