High-stability hollow fibrous membrane and preparation method thereof
A high-stability, fiber-membrane technology, applied in the field of composite materials, can solve problems such as poor stability, low retention rate, and poor tensile strength, and achieve the effects of improved stability, simple process, and easy control
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[0021] Example 1
[0022] A high-stability hollow fiber membrane includes polyvinylidene fluoride membrane filaments, and cross-linked products are uniformly inlaid inside the polyvinylidene fluoride membrane filaments and the pores. The cross-linked product is formed by cross-linking polyvinyl alcohol and glutaraldehyde.
[0023] A method for preparing hollow fiber membranes with high stability, such as figure 1 The process flow shown includes the following steps:
[0024] 1) Prepare polyvinyl alcohol and water into an aqueous solution of polyvinyl alcohol with a concentration of 15% by mass;
[0025] 2) Take 30g of polyvinyl alcohol aqueous solution and add it to 500ml of dimethylacetamide, maintain the temperature at 65°C, stir evenly, then add 150g of polyvinylidene fluoride powder, continue to maintain the temperature at 65°C and stir evenly;
[0026] 3) Add 20g of the pore-forming agent PVP and 10g of the surfactant Tween 80 to the mixture obtained in step 2), stir evenly and po...
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[0034] Example 2
[0035] A high-stability hollow fiber membrane includes polyvinylidene fluoride membrane filaments, and cross-linked products are uniformly inlaid inside the polyvinylidene fluoride membrane filaments and the pores. The cross-linked product is formed by cross-linking polyvinyl alcohol and glutaraldehyde.
[0036] A method for preparing hollow fiber membranes with high stability, such as figure 1 The process flow shown includes the following steps:
[0037] 1) Prepare polyvinyl alcohol and water into a polyvinyl alcohol aqueous solution with a concentration of 18% by mass;
[0038] 2) Take 40g of polyvinyl alcohol aqueous solution and add it to 500ml of dimethylacetamide, maintain the temperature at 75℃, stir well, then add 160g of polyvinylidene fluoride powder, continue to maintain the temperature at 75℃ and stir evenly;
[0039] 3) Add 40g of the pore-forming agent PVP and 20g of the surfactant Tween 80 to the mixture obtained in step 2), stir evenly and pour it in...
Example Embodiment
[0046] Example 3
[0047] A high-stability hollow fiber membrane comprises polyvinylidene fluoride membrane filaments, and cross-linked products are uniformly inlaid in the inside and pores of the polyvinylidene fluoride membrane filaments. The cross-linked product is formed by cross-linking polyvinyl alcohol and glutaraldehyde.
[0048] A method for preparing hollow fiber membranes with high stability, such as figure 1 The process flow shown includes the following steps:
[0049] 1) Prepare polyvinyl alcohol and water into an aqueous solution of polyvinyl alcohol with a concentration of 14% by mass;
[0050] 2) Take 35g of polyvinyl alcohol aqueous solution and add it to 500ml of dimethylacetamide, maintain the temperature at 85°C, stir evenly, then add 170g of polyvinylidene fluoride powder, continue to maintain the temperature at 85°C and stir evenly;
[0051] 3) Add 30g of the pore-forming agent PVP and 15g of the surfactant Tween 80 to the mixture obtained in step 2), stir evenly...
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