Ultraviolet excited green fluorescent inkjet ink for printing and imaging by additive method and preparation method
A green fluorescent, ink-jet ink technology, applied in inks, applications, household appliances, etc., can solve the problems of complex process and can not meet the needs of modern life, and achieve the effect of simple preparation process, good anti-counterfeiting effect, and obvious effect.
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Embodiment 1
[0035] Add 0.5 parts of UV-excited green to 13.5 parts of dimethyl sulfoxide (analytical pure), 31.5 parts of methyl acetate (analytical pure): butyl ester (analytical pure) in a mixed ester solvent of 1:4 (weight ratio) Fluorescent anti-counterfeiting material (hereinafter referred to as green fluorescent material), heated magnetically and stirred evenly at 30°C, stirred for 45 minutes to form component A; added 11 parts of N,N-methyl formazan to 15.5 parts of epoxy resin (commercially available) Amide (analytical pure), 26.5 parts of propylene glycol methyl ether (analytical pure) ether solvent, in which synthetic resin is, after magnetic stirring evenly, component B is formed, components A and B are mixed and stirred for 30 minutes until the solution is completely transparent, add 1 part Organic fluorine surfactant (TEGO), 0.5 parts of pH regulator triethanolamine (analytical pure). Mix and stir for 20 minutes to obtain the ink, which can be spray-painted on the substrate. ...
Embodiment 2
[0040] Add 3.5 parts of green fluorescent material to 17.5 parts of sulfolane (analytical pure) and 34.5 parts of propylene glycol methyl ether acetate (analytical pure), heat and magnetically stir evenly at a temperature of 55 ° C, and stir for 50 minutes to form A component; add 15.5 parts Add 13.5 parts of N,N-methylacetamide (analytical pure) and 17 parts of ethylene glycol ethyl ether (analytical pure) to polyurethane resin (commercially available), and stir magnetically for 30 minutes to form component B, components A and B Mix and stir for 40 minutes until the solution is completely transparent, add 1 part of silicone surfactant (TEGO) and 1 part of pH regulator triethylamine (analytical pure). Mix and stir for 25 minutes to obtain the ink, which can be spray-painted on the substrate.
Embodiment 3
[0042] Add 5 parts of green fluorescent material to 20 parts of sulfolane (analytically pure) and 15 parts of propylene glycol methyl ether acetate (analytical pure), heat and magnetically stir evenly at a temperature of 45°C, and stir for 60 minutes to form A component; add 19.5 parts Add 21.5 parts of ethylene glycol ether (analytical grade) and 19 parts of diethylene glycol butyl ether: 1,4-dioxane in a mixed ether solvent of 3:2 (weight ratio) to polyurethane resin (commercially available). After magnetically stirring for 30 minutes to form component B, mix and stir components A and B for 60 minutes until the solution is completely transparent, then add 2 parts of organic fluorine surfactant (TEGO) and 1 part of pH regulator N,N-dimethylformamide (analytical pure). Mix and stir for 10 minutes to obtain the ink, which can be spray-painted on the substrate.
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Abstract
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