Urea-based lubricating grease composition
A technology of urea-based grease and composition, applied in the field of grease, can solve the problems of inability to use for a long time, lubricating performance, decline in anti-wear extreme pressure performance, lack of extreme pressure and wear resistance, etc., and achieve long-term service life and long-term stability. long-term, excellent lubricity
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Embodiment 1
[0030] Mix the raw materials according to the following weight
[0031] 150BS mechanical oil: 840kg, No. 100 mechanical oil: 210kg,
[0032] p-phenylenediamine: 30kg, cyclohexylamine: 70kg,
[0033] Diphenylamine: 7.5kg, MDI (100): 300kg,
[0034] Molybdenum carbonophosphate (T300): 30kg, primary alkyl zinc dithiophosphate (T202): 6kg;
[0035] Production method: (1) Put 20% of the total weight of base oil into the first reaction kettle, heat to 50°C, then add p-toluidine, stir and heat to 80°C, stop stirring for later use.
[0036] (2) Put the remaining base oil into the second reaction kettle and heat up to 5°C, then add MDI (100), stir and heat up to 78°C; at the same time, add cyclohexylamine to the first reaction kettle and stir for 15 minutes, Then add it all to the second reaction kettle.
[0037] (3) Stir and heat up to 130° C., then stop stirring for 5 minutes and then stir for 5 minutes, and repeat this 3 times.
[0038] (4) Keep the temperature above 130°C, tra...
Embodiment 2
[0041] Mix the raw materials according to the following weight
[0042] 150BS mechanical oil: 900kg, No. 100 mechanical oil: 225kg,
[0043] p-phenylenediamine: 45kg, cyclohexylamine: 45kg,
[0044] Diphenylamine: 3kg, MDI (100): 150kg,
[0045] Molybdenum carbonophosphate (T300): 75kg, primary alkyl zinc dithiophosphate (T202): 15kg;
[0046] Production method: (1) Put 40% of the total weight of base oil into the first reaction kettle, heat to 55°C, then add p-toluidine, stir and heat to 85°C, stop stirring for later use.
[0047] (2) Put the remaining base oil into the second reaction kettle and heat up to 5°C, then add MDI (100), stir and raise the temperature to 75°C; at the same time, add cyclohexylamine to the first reaction kettle and stir for 13 minutes, Then add it all to the second reaction kettle.
[0048] (3) Stir and heat up to 130° C., then stop stirring for 5 minutes and then stir for 5 minutes, and repeat this 3 times.
[0049] (4) Keep the temperature above...
Embodiment 3
[0051] Mix the raw materials according to the following weight
[0052] 150BS mechanical oil: 675kg, No. 100 mechanical oil: 450kg,
[0053] p-phenylenediamine: 30kg, cyclohexylamine: 90kg,
[0054] Diphenylamine: 9kg, MDI (100): 270kg,
[0055] Molybdenum carbonophosphate (T300): 30kg, primary alkyl zinc dithiophosphate (T202): 30kg;
[0056] Production method: (1) Put 70% of the total weight of base oil into the first reaction kettle, heat to 55°C, then add p-toluidine, stir and heat to 85°C, stop stirring for later use.
[0057] (2) Put the remaining base oil into the second reaction kettle and heat up to 5°C, then add MDI (100), stir and raise the temperature to 77°C; at the same time, add cyclohexylamine to the first reaction kettle and stir for 15 minutes, Then add it all to the second reaction kettle.
[0058] (3) Stir and heat up to 130° C., then stop stirring for 5 minutes and then stir for 5 minutes, and repeat this 3 times.
[0059] (4) Keep the temperature abo...
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