Cationic type polypropylene carbonate waterborne polyurethane emulsion as well as preparation method and application
A technology of polypropylene carbonate and water-based polyurethane, applied in the field of water-based polyurethane, which can solve the problems of poor water resistance, limited practical performance, and low mechanical strength of cationic water-based polyurethane, and achieve excellent adhesion, enhanced fiber strength and pressure, and penetration Good performance of sex and adhesion
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Example Embodiment
[0025] Example 1
[0026] Each component is operated according to the following steps: 65 parts by mass of polypropylene carbonate polyol and 25 parts by mass of IPDI are added into a three-necked flask with an electric stirring device and mixed, the temperature is raised to 60° C., 0.8 parts by mass of DBTDL is added, and gradually The temperature was raised to 85°C, and the reaction was kept for 2 hours; the temperature was lowered to 40°C, 6.7 parts by mass of N-methyldiethanolamine was slowly added dropwise, and the reaction was carried out for 3 hours; acetone to adjust the viscosity to prevent gel formation due to excessive viscosity; when the temperature drops to 35-45°C, add 3 parts by mass of acetic acid to react for 0.5 h; add 250 parts by mass of deionized water to emulsify, stir at high speed for 1 h, evaporate the acetone, The cationic polypropylene carbonate aqueous polyurethane emulsion is obtained.
[0027] After the obtained emulsion was formed into a film an...
Example Embodiment
[0028] Example 2
[0029] Each component is operated according to the following steps: 65 parts by mass of polypropylene carbonate polyol and 25 parts by mass of IPDI are added into a three-necked flask with an electric stirring device and mixed, the temperature is raised to 60° C., 0.8 parts by mass of DBTDL is added, and gradually The temperature was raised to 85°C, and the reaction was incubated for 2 hours; the temperature was lowered to 40°C, and 6 parts by mass of N-methyldiethanolamine were slowly added dropwise for 3 hours; the temperature was raised to 60°C, 2 parts by mass of glycerol were added, and the reaction was performed for 1 hour; 100 parts by mass of acetone was used to adjust the viscosity to prevent the formation of gel due to excessive viscosity; when the temperature dropped to 35-45°C, 2.8 parts by mass of acetic acid was added to react for 0.5 h; Acetone is used to obtain cationic polypropylene carbonate aqueous polyurethane emulsion.
[0030] After th...
Example Embodiment
[0031] Example 3
[0032] Each component is operated according to the following steps: 65 parts by mass of polypropylene carbonate polyol and 25 parts by mass of IPDI are added into a three-necked flask with an electric stirring device and mixed, the temperature is raised to 60° C., 0.8 parts by mass of DBTDL is added, and gradually The temperature was raised to 85°C, and the reaction was kept for 2 hours; the temperature was lowered to 40°C, 6.5 parts by mass of N-methyldiethanolamine was slowly added dropwise, and the reaction was carried out for 3 hours; ; Add 80-100 parts by mass of acetone to adjust the viscosity to prevent the formation of gel due to excessive viscosity; when the temperature drops to 35-45 ℃, add 3 parts by mass of acetic acid to react for 0.5h; add 250 parts by mass of deionized water to emulsify and stir at high speed For 1 h, the acetone was evaporated to obtain a cationic polypropylene carbonate aqueous polyurethane emulsion.
[0033] After the obta...
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