Preparation method of polypeptide soybean protein complex fiber
A soybean protein and composite fiber technology, which is applied in the chemical characteristics of fibers, cellulose/protein conjugated rayon, and rayon manufacturing, etc., can solve the problem of lack of low molecular protein activity, penetration, specificity and regulation. , low biological activity of high molecular weight proteins, affecting the protein cavity structure and other problems, to achieve the effect of improving binding stability, simplifying production steps, and not easy to lose
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Embodiment 1
[0026] Embodiment 1 prepares 1.67dtex * 38mm polypeptide soybean protein composite fiber
[0027] Soak the soybean protein in a sodium hydroxide solution with a concentration of 20wt%, stir at a high speed to obtain a soybean protein solution, filter the soybean protein solution to remove impurities, and then add 2.5wt% of a dispersant in the soybean protein solution, The pH value of the soybean protein solution is adjusted to 6.5, and then an ultrafiltration membrane with an average molecular weight of 8000-10000 is used for ultrafiltration dialysis to obtain a polypeptide soybean protein mother liquor with an average molecular weight of 1800.
[0028] Soaking polyvinyl alcohol in water, dissolving, and filtering to obtain a polyvinyl alcohol solution, adding the polypeptide soybean protein mother liquor to the polyvinyl alcohol solution according to the ratio of the protein content in the polyvinyl alcohol to 20 wt%, and then Adding acrylic acid as a crosslinking agent accou...
Embodiment 2
[0031] Example 2 Preparation of 1.67dtex × 38mm Polypeptide Soybean Protein Composite Fiber
[0032]Soak the soybean protein in the dilute alkali solution and react for 4 hours at a temperature of 80°C. The bath ratio of the soybean protein to the dilute alkali solution is 20:60. After stirring at a speed of 100 rpm for 0.5 to 1 hour The soybean protein solution is obtained. After filtering the soybean protein solution to remove impurities, add a dispersant with a concentration of 1.5wt% in the soybean protein solution, adjust the pH value of the soybean protein solution to 7.0, and then use an ultra- The filter membrane is subjected to ultrafiltration and dialysis to obtain a polypeptide soybean protein mother liquor with an average protein molecular weight of 2000.
[0033] Soaking polyvinyl alcohol in water, dissolving, and filtering to obtain a polyvinyl alcohol solution, adding the polypeptide soybean protein mother liquor to the polyvinyl alcohol solution according to t...
Embodiment 3
[0036] Example 3 Preparation of 1.33dtex × 38mm Polypeptide Soybean Protein Composite Fiber
[0037] Soak the soybean protein in the dilute alkali solution and react for 3 hours at a temperature of 100°C. The bath ratio of the soybean protein to the dilute alkali solution is 30:70. After stirring at a speed of 150 rpm for 0.5 hours, the obtained The soy protein solution described above. After filtering the soybean protein solution to remove impurities, add a dispersant with a concentration of 5wt% in the soybean protein solution, adjust the pH value of the soybean protein solution to 6.8, and then use an ultrafiltration filter with an average molecular weight of 8000 The membrane is subjected to ultrafiltration and dialysis to obtain a polypeptide soybean protein mother liquor with an average protein molecular weight of 500.
[0038] The polyvinyl alcohol is soaked, dissolved, and filtered to obtain a polyvinyl alcohol solution, and the polypeptide soybean protein mother liqu...
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