Gluten fiber preparation method
A gluten and fiber technology, which is used in the preparation of protein fibers and the field of protein fiber preparation, can solve the problems of low fiber protein content, complicated production process, and fiber strength cannot be guaranteed, and achieves good biocompatibility and tensile mechanics. Good performance and the effect of filling the demand gap
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Embodiment 1
[0027] (1) Preparation of spinning solution
[0028] Dissolve 100Kg of gluten powder in a urea solution whose mass is 3 times that of gluten powder, stir well and leave the solution temperature at 40°C for 12 hours to obtain a spinning solution; the molar concentration of the urea solution is 9mol / L, the urea solution containing mass percent concentration is 1% Na 2 SO 3 reducing agent;
[0029] (2), wet spinning
[0030] The spinning solution obtained in step (1) is stretched and spun under the condition of 70° C. to obtain preliminary silky gluten strands;
[0031] (3), solidification
[0032] At normal temperature, the preliminary filamentous gluten strips prepared in step (2) were immersed in Na 2 SO 4 Preliminary coagulation is carried out in the solution, and the coagulation time is 30min to obtain coagulated gluten filaments; Na 2 SO 4 The mass percentage concentration of solution is 8%; 2 SO 4 The mass ratio of the solution is 1:6;
[0033] (4), citric aci...
Embodiment 2
[0040] (1) Preparation of spinning solution
[0041] Dissolve 100Kg of gluten powder in a urea solution whose mass is 4 times that of gluten powder, stir well and then make the solution temperature be 50°C and leave it to stand for 10 hours in a sealed condition to obtain spinning solution; wherein the molar concentration of urea solution is 9mol / L, the urea solution containing mass percent concentration is 0.8% Na 2 SO 3 reducing agent;
[0042] (2), wet spinning
[0043] The spinning solution obtained in step (1) is stretched and spun under the condition of 80° C. to obtain preliminary silky gluten strands;
[0044] (3), solidification
[0045] At normal temperature, the preliminary filamentous gluten strips prepared in step (2) were immersed in Na2 SO 4 Preliminary coagulation is carried out in the solution, and the coagulation time is 15min to obtain coagulated gluten filaments; Na 2 SO 4 The mass percentage concentration of solution is 10%; 2 SO 4 The mass rati...
Embodiment 3
[0053] (1) Preparation of spinning solution
[0054] 100Kg gluten powder is dissolved in the urea solution that quality is 5 times of gluten powder, after fully stirring evenly, make solution temperature be 20 ℃ of conditions and seal and stand for 40h, obtain spinning solution; Wherein the molar concentration of urea solution is 9mol / L, the urea solution containing mass percent concentration is 1.5% Na 2 SO 3 reducing agent;
[0055] (2), wet spinning
[0056] The spinning solution obtained in step (1) is stretched and spun under the condition of 90° C. to obtain preliminary silky gluten strands;
[0057] (3), solidification
[0058] At normal temperature, the preliminary filamentous gluten strips prepared in step (2) were immersed in Na 2 SO 4 Preliminary coagulation is carried out in the solution, and the coagulation time is 45min to obtain coagulated gluten filaments; Na 2 SO 4 The mass percentage concentration of solution is 15%; 2 SO 4 The mass ratio of the s...
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