Preparation method of magnesium aluminum lanthanum type hydrotalcite PVC composite heat stabilizer
A composite thermal stabilizer, hydrotalcite technology, applied in chemical instruments and methods, rare earth metal compounds, inorganic chemistry, etc., can solve the problems of pollution, high cost, complicated preparation process, etc., and achieve simplified steps and good thermal stability effect. , the effect of simple preparation process
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[0013] Magnesium-aluminum-lanthanum hydrotalcite was synthesized by heating precipitation. Specific examples are as follows:
[0014] 1) Weigh 5.12 g of magnesium nitrate, 2.25 g of aluminum nitrate and 1.73 g of lanthanum nitrate, dissolve in 50 mL of distilled water to make mixed solution A, preheat to 80 °C; take 2.86 g of sodium hydroxide and 1.06 g of anhydrous sodium carbonate to dissolve Prepare mixed solution B in 50mL distilled water, preheat to 80 °C;
[0015] 2) Preheat 50mL of distilled water in a 250mL three-neck flask and preheat to 80 °C;
[0016] 3) Pour the mixture A and B into the three-neck flask in the step and stir vigorously for 2 h;
[0017] 4) After the stirring was stopped, the slurry was allowed to stand at 90 °C for 24 h to crystallize;
[0018] 5) Filter the crystallized hydrotalcite slurry at 90 °C and wash it thoroughly with hot water until the filtrate is PH<8;
[0019] 6) Dry the filter cake in step 5) at 80°C, and then seal it for storag...
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