Process for the production of hydroxylamine by reduction of nitrate or nitrogen monoxide
A technology for producing hydroxylamine and nitric oxide, applied in chemical instruments and methods, preparation of hydroxylamine and lactam, etc., can solve the problems of increasing the variable cost of hydroxylamine, consuming ion exchange resin, increasing the required input, etc. The effect of energy consumption, reduction of raw material consumption, and reduction of energy consumption
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[0064] The present invention is illustrated by the following examples, but is not limited thereto.
[0065] This experiment was performed in a commercial cyclohexanone oxime facility, according to process to operate. Continuous and selective reduction of nitrate with hydrogen produces hydroxylamine. The prepared hydroxylamine is converted to cyclohexanone oxime by reaction with cyclohexanone in the oximation zone. The structure is mainly as figure 1 shown.
[0066] The apparatus includes a hydroxylamine-forming zone where nitrates in an aqueous phosphate buffer solution are reduced. Using heterogeneous catalyst Pd / C and adding promoter GeO 2. The output of the partially phosphate-containing acidic aqueous solution also containing hydroxylamine is continued and added to the oximation zone after filtration to remove the catalyst. The aqueous hydroxylamine solution is contacted with cyclohexanone dissolved in toluene in the oximation zone. The oximati...
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