Polyester alkali decrement and one-bath-dyeing one-step low-temperature processing method

A processing method and alkali weight reduction technology, which is applied in the field of dyeing and finishing, can solve the problems of lowering the dyeing temperature of polyester disperse dyes, high energy and chemical consumption, unfavorable energy saving and emission reduction, etc., so as to improve processing efficiency, reduce consumption, and facilitate operation Effect

Active Publication Date: 2014-02-19
绍兴通盛印染有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The technical problem to be solved by the present invention is that the polyester alkali weight reduction and dyeing process need to be carried out in two steps, and it needs to be carried out under the conditions of higher temperature and higher chemical consumption, and there are complex processes, large energy and chemical consumption, and Disadvantages that are not conducive to energy saving, emissi...

Method used

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  • Polyester alkali decrement and one-bath-dyeing one-step low-temperature processing method

Examples

Experimental program
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Effect test

Embodiment 1

[0015] A one-bath low-temperature processing method for polyester alkali weight reduction and dyeing. The polyester is subjected to one-bath alkali weight reduction dyeing and one-step processing by dipping technology. The processing process is as follows: sodium hydroxide, cationic accelerator 1227 (dodecyl Methyl benzyl ammonium chloride), carrier benzyl alcohol, dispersant DN and disperse orange BROB were dissolved in water to prepare a dye liquor, and then the polyester fabric was put into the dye liquor with a bath ratio of 1:40, and then the dye was dyed at 1°C / min The heating rate was raised to 95°C, and the temperature was kept for 50 minutes. After the heat preservation, the polyester fabric was taken out and washed twice with tap water, and then reduced and cleaned with 2g / L sodium hydroxide and 2g / L sodium hydroxide at 70°C with a bath ratio of 1:50. After 10 minutes, take out the fabric and wash it with water for 6 times, and finally dry the fabric at 80°C.

[0016...

Embodiment 2

[0023] A one-bath low-temperature processing method for polyester alkali weight reduction and dyeing. The polyester is processed by dipping technology in one bath for alkali weight reduction and dyeing. The processing process is as follows: sodium hydroxide, cationic accelerator 1631 (cetyl tri Methyl ammonium bromide), carrier JYK POW, dispersant DN and disperse red 902 were dissolved in water to prepare a dye liquor, and then the polyester fabric was put into the dye liquor with a liquor ratio of 1:20, and then the temperature was raised at 1.5°C / min Raise the temperature to 98°C and keep it warm for 40 minutes. After the heat preservation is over, take out the polyester fabric and wash it with tap water for 5 times, and then use 2g / L sodium hydroxide and 2g / L sodium hydroxide to reduce and wash it for 10 minutes at 75°C with a bath ratio of 1:50. Then take out the fabric and wash it twice with water, and finally dry the fabric at 70°C.

[0024] The dye solution prescription...

Embodiment 3

[0031] A one-bath low-temperature processing method for polyester alkali weight reduction and dyeing. The dipping process is used to perform alkali weight reduction dyeing of polyester in one bath. The processing process is as follows: sodium hydroxide, cationic accelerator SN (octadecyl Methyl hydroxyethyl quaternary ammonium nitrate), carrier TF-258, dispersant DN and disperse blue 825 were dissolved in water to prepare a dye solution, and then the polyester fabric was put into the dye solution with a bath ratio of 1:10, and then 2 The heating rate of ℃ / min is raised to 100 ℃, and the temperature is kept for 30 minutes. After the heat preservation is completed, the polyester fabric is taken out and washed 3 times with tap water, and then 2g / L sodium hydroxide and 2g / L sodium hydroxide are used at 80 ℃ with a bath ratio of 1:50. Reduce and wash for 10 minutes, then take out the fabric and wash it with water for 4 times, and finally dry the fabric at 75°C.

[0032]

[0033] T...

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Abstract

The invention discloses a polyester alkali decrement and one-bath-dyeing one-step low-temperature processing method. The method comprises the steps: carrying out alkali decrement and one-bath-dyeing one-step processing on polyester by using a dipping process, and dissolving sodium hydroxide, a cation accelerant, a carrier, a dispersing agent and a disperse dye into a dye liquid, wherein the dye liquid is prepared from water, the concentration of the carrier is 4-15g/L, the concentration of the sodium hydroxide is 2-4g/L, and the concentration of the cation accelerant is 1*10<-5> to 10*10<-5>mol/L; placing a polyester fabric into the dye liquid according to the bath ratio of 1: (10-100); then, heating to 90-100 DEG C at the speed of 0.5-2 DEG C/min, preserving the heat for 20-100min; taking out the polyester fabric after the heat preservation is ended, washing the polyester fabric 2-5 times by using tap water, and then, carrying out reduction clearing at the temperature of 70-80 DEG C and the bath ratio of 1:50 for 10min by using 2g/L sodium hydroxide and 2g/L sodium hydrosulfite; next, taking out the fabric, and washing 2-6 times by using water; and finally, drying the fabric at the temperature of 70-80 DEG C. By using the method, the polyester alkali decrement and dyeing processing flow is shortened, the alkali decrement processing temperature is reduced, the consumptions of the sodium hydroxide and the cation accelerant are reduced, the production efficiency is increased, the energy sources are saved, the process is simple, no special requirement for the polyester fabric and equipment are needed, and the large-scale production can be realized by using conventional equipment, so that the method has a wide application prospect.

Description

technical field [0001] The invention belongs to the technical field of dyeing and finishing, and relates to a one-bath, one-step low-temperature processing for alkali weight reduction and dyeing of polyester by adding a carrier for dyeing polyester disperse dyes into a treatment solution. Background technique [0002] Polyester is the synthetic fiber with the largest output in the world. It has good dyeing performance, high strength, quick drying, and is not easy to wrinkle. It is suitable for manufacturing various clothing fabrics. In order to increase the added value of polyester fabrics, people have developed an alkali weight reduction process to produce imitation silk polyester. At present, the alkali weight reduction and dyeing of polyester usually adopt a two-step process, and the products produced have excellent performance; however, the disadvantages of the two-step process are that the process is relatively long and consumes a lot of energy. In 2012, Wang Chao publ...

Claims

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Application Information

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IPC IPC(8): D06P3/54D06P1/16D06P1/651D06P1/44
Inventor 曹机良盛杰侦孟春丽王延伟曹毅翟圣国潘星远
Owner 绍兴通盛印染有限公司
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