Method for rapidly evaluating adsorption effect of porous filter tip additive
An additive and porosity technology, which is applied in the field of rapid evaluation of the adsorption effect of porous filter additives, can solve the problems of large waste, high cost, inconsistent filter adding methods (evenly distributed in acetate fibers, etc.), and achieve high test sensitivity and operation Simple, step-saving and cost-effective
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Embodiment 1
[0027] The toxic substance is n-butyraldehyde, and the porous filter additives to be evaluated are powdered additive 1 (molecular sieve), additive 2 (molecular sieve), and additive 3 (micro-medium composite porous material).
[0028] (1) Preliminary degassing of additives: Weigh 150-200 mg of the above three additives and degas at 180°C overnight with a specific surface area meter to preliminarily remove the impurity gases in the filter additives.
[0029] (2) Transfer 5-15ml of n-butyraldehyde liquid to the vaporization storage tank, weigh 50-100mg of the filter additive after preliminary degassing treatment, and install it into the quartz hanging basket of the intelligent weight absorption instrument.
[0030] (3) Secondary degassing: Heat the sample to 180°C through the external heating device, keep it for 4 hours, and use the vacuum pump to further remove the residual impurity gas in the additive.
[0031] (4) Adsorption: According to the saturated vapor pressure of the selected or...
Embodiment 2
[0042] The toxic substance is selected as benzene, and the filter additives to be evaluated are powdered additive 4 (molecular sieve) and additive 5 (micro-mesoporous material) for their adsorption effect on benzene series.
[0043] (1) Preliminary degassing of additives: Weigh 150-200 mg of the above two additives respectively, and degas at 180°C overnight with a surface area meter to preliminarily remove the impurity gases in the filter additives.
[0044] (2 Transfer 5-15ml of benzene liquid to the vaporization storage tank, weigh 50-100mg of the filter additive after preliminary degassing treatment, and install it into the quartz hanging basket of the intelligent weight absorption meter.
[0045] (3) Secondary degassing: Heat the sample to 180°C through an external heating device, keep it for 4 hours, and use a vacuum pump to further remove the residual impurity gas in the additive.
[0046] (4) Adsorption: According to the saturated vapor pressure of the selected organic liquid or...
Embodiment 3
[0056] The toxic substance is selected as CO, and the filter additives to be evaluated are powdered additive 6 (molecular sieve) and additive 7 (micro-mesoporous material) for the adsorption effect of CO.
[0057] (1) Preliminary degassing of additives: Weigh 150-200 mg of the above two additives respectively, and degas at 180°C overnight with a surface area meter to preliminarily remove the impurity gases in the filter additives.
[0058] (2) Connect the CO gas bottle to the intelligent adsorption instrument, weigh 50-100mg of the filter additive after preliminary degassing treatment, and install it into the quartz hanging basket of the intelligent weight absorption instrument.
[0059] (3) Secondary degassing: Heat the sample to 180°C through the external heating device, keep it for 4 hours, and use the vacuum pump to further remove the residual impurity gas in the additive.
[0060] (4) Adsorption: According to the saturated vapor pressure of the selected gas, 27 test pressure point...
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