Phase change ink composition and conductive pattern formed from the composition
A phase change ink and composition technology, which is applied to inks, conductive materials dispersed in non-conductive inorganic materials, household appliances, etc., can solve the problems of inability to mix polar additives, only dissolve, phase separation, etc. Storage stability, anti-settling effect
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[0055] Hereinafter, to help understand the present invention, preferred embodiments will be provided. However, these embodiments are provided for easier understanding of the present invention, and should not be construed as limiting the scope of the present invention described herein.
[0056] 1. Preparation of ink composition
preparation example 1-E1
[0058] 50g of ethylene glycol (boiling point of 197°C) solution containing 50wt% of silver nanoparticles covered with polyvinylpyrrolidone (synthesized by polyol synthesis) and 25g of dimethyl sulfone were mixed to prepare a mixture, and the prepared mixture Put it into a nitrogen-circulating flask and heat to 200°C while stirring with a magnetic bar. At this time, the dimethyl sulfone is melted and uniformly mixed with the solution containing silver nanoparticles. As the heating continues, ethylene glycol (which is a relatively low boiling solvent originally contained in the solution containing silver nanoparticles) is evaporated. Continue heating for 1 hour to prepare a composition containing about 25 g of silver nanoparticles, about 25 g of dimethyl sulfone and other materials. 100 parts by weight of the prepared ink composition consisted of 45 parts by weight of silver nanoparticles adsorbed with polyvinylpyrrolidone, 3 parts by weight of polyvinylpyrrolidone, and 52 parts...
preparation example 2-E2
[0060] A centrifugal process was performed on a dispersion containing silver nanoparticles (synthesized by polyol synthesis) covered with polyvinylpyrrolidone to prepare 25 g of silver paste. The obtained silver paste was mixed with 55 g of sulfolane to prepare a mixture, and then the prepared mixture was put into a flask in which nitrogen gas was flowed, and heated to 150° C. while stirring with a magnetic bar. 100 parts by weight of the prepared ink composition consisted of 32 parts by weight of silver nanoparticles, 2 parts by weight of polyvinylpyrrolidone, and 66 parts by weight of sulfolane. The ink composition is cured at about 25°C and is liquid or semi-solid at room temperature.
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