Copper powder surface activity activating technology in copper steel bimetal powder sintering
A surface-active, bimetallic technology, applied in the field of powder metallurgy sintering, can solve the problem of weak bonding strength between copper alloy and steel back, and achieve the effect of reducing activation energy and enhancing bonding strength
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Embodiment 1
[0038] 1. Preparation before sintering
[0039] 1.1 Raw material and ratio:
[0040] Copper 80wt%, tin 10wt%, lead 10wt%.
[0041] 1.2 Mixing parameters:
[0042] First mix copper powder and tin powder for one hour, then add lead powder and mix for one hour.
[0043] 1.3 Arrange corundum rings on the burning boat, put the steel back after cyanide copper plating into the corundum ring, loosely spread powder until the steel back is covered, and press firmly. Here, the initial firing is not to obtain a dense structure, but to obtain a higher binding force.
[0044] 2 Activate the copper powder surface activity of the product
[0045] 2.1 Put the copper-steel bimetallic powder sintered sample in the furnace, and heat it from room temperature to 260°C at a rate of 6°C / min without protective gas;
[0046] 2.2 Start to feed nitrogen into the furnace, the flow rate is 200L / h, and keep warm for 20 minutes;
[0047] 2.3 After the heat preservation is over, the temperature is raise...
Embodiment 2
[0055] 1. Preparation before sintering
[0056] Same as step 1 in Example 1.
[0057] 2 Activate the copper powder surface activity of the product
[0058] 2.1 Put the copper-steel bimetallic powder sintered sample in the furnace, and heat it from room temperature to 300°C at a rate of 6°C / min without protective gas;
[0059] 2.2 Start to feed nitrogen into the furnace, the flow rate is 200L / h, and keep warm for 30 minutes;
[0060] 2.3 After the heat preservation is over, the temperature is raised to 450°C, and the heating rate is 4°C / min;
[0061] 2.4 Continue heating and feed hydrogen gas at a flow rate of 80L / h. After 30 minutes, the nitrogen flow rate is reduced to 140L / h. At the same time, heat to 850°C with a heating rate of 4°C / min;
[0062] 2.5 After 30 minutes of heat preservation, the furnace is cooled to room temperature under a protective atmosphere.
[0063] 2.6 After the sample is taken out, the re-compression and re-firing process is carried out. The re-fir...
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