Method for leaching positive-negative pole material mixture of waste nickel-metal hydride battery
A technology for nickel-hydrogen waste batteries and mixed materials, which is applied in the direction of improving process efficiency, can solve the problems of uneconomical self-use of industrial pure oxygen, complicated leaching equipment, and small amount of industrial pure oxygen, etc., and achieves obvious economic and environmental benefits. , the effect of reducing pollution control costs and improving metal leaching rate
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Embodiment 1
[0014] Example 1: Add 100 g of the positive and negative mixed materials of spent nickel-metal hydride batteries (containing 55.3% nickel, 6.2% cobalt, and 12.5% rare earth) through roasting pretreatment into a stainless steel pressure reactor with a volume of 1 L, and add 1.5 mol / L 950ml of sulfuric acid, stirred at 40℃~50℃ (stirring speed 80r / min) into SO 2 After leaching for 2.5 hours, the leaching pressure was 0.05 MPa. After the leaching, liquid-solid separation was carried out to obtain 910ml of leaching solution (excluding leaching slag washing water). The leaching rates of nickel, cobalt and rare earth are 99.0%, 98.0% and 9.7% respectively (calculated based on the nickel, cobalt and rare earth entering the leaching solution and leaching slag washing solution).
Embodiment 2
[0015] Example 2: Add 500 g of mixed positive and negative electrode materials (containing 55.3% nickel, 6.2% cobalt, and 12.5% rare earth) of waste nickel-metal hydride batteries (containing 55.3% nickel, 6.2% cobalt, and 12.5% rare earth) that have been pretreated by roasting into a stainless steel pressure reactor with a volume of 5 L, and add 2.0 mol / L 3800ml of sulfuric acid, stirred at 40 ℃ ~ 50 ℃ (stirring speed 80r / min) into SO 2 After leaching for 2.0 hours, the leaching pressure was 0.07MPa. After the leaching, liquid-solid separation was carried out to obtain 3600ml leaching solution (excluding leaching slag washing water). The leaching rates of nickel, cobalt and rare earths are 99.3%, 98.5% and 8.2% respectively (calculated based on nickel, cobalt and rare earths entering the leaching solution and leaching slag washing solution).
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