High-pressure high-temperature liquid viscosity measuring device and method

A high-temperature, high-pressure, and liquid-viscosity technology, applied in the direction of measuring devices, flow characteristics, instruments, etc., can solve problems such as increased system resistance, instability, and changes in the rheological properties of oil-coal slurry, so as to improve the sealing performance of the system and ensure uniformity , good reproducibility

Active Publication Date: 2014-04-30
CCTEG CHINA COAL RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

In the direct coal liquefaction process, after the high-concentration oil-coal slurry passes through the preheater, its temperature will rise to about 400°C. At this time, some bridge bonds between the coal structural units have broken, thus generating free radicals , free radicals are very unstable, if there is no high-pressure hydrogen environment and the separation of solvent molecules, free radicals wil

Method used

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  • High-pressure high-temperature liquid viscosity measuring device and method
  • High-pressure high-temperature liquid viscosity measuring device and method
  • High-pressure high-temperature liquid viscosity measuring device and method

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Embodiment 1

[0036] Such as figure 1 As shown, an embodiment of the present invention proposes a high-temperature and high-pressure liquid viscosity measurement device, which includes a high-temperature and high-pressure system and a measurement system. The high-temperature and high-pressure system is used to accommodate liquids and provide high-temperature and high-pressure environments for liquids, which can be A closed high-temperature and high-pressure reactor with a function of heating and pressurizing; the measurement system includes a drive motor 1, a torque sensor 2, a drive magnetic cylinder 3, an induction magnetic cylinder 12, a rotating shaft 21 and a stirring paddle 20; the drive motor 1 and The upper end of the torque sensor 2 is connected to provide driving force for the torque sensor 2, so that it drives the assembly connected to its lower end to rotate. In the embodiment of the present invention, a portable micro-motor is selected; the lower end of the torque sensor 2 It i...

Embodiment 2

[0047] An embodiment of the present invention provides a method for measuring the viscosity of a high-temperature and high-pressure liquid. The measuring method uses the high-temperature and high-pressure liquid viscosity measuring device provided in the above-mentioned embodiment for measurement. The measuring method includes the following steps:

[0048] Step 1: adding liquid into the high temperature and high pressure system, making it submerge the stirring paddle 20;

[0049] The liquid described in the embodiment of the present invention is oil-coal slurry, and the oil-coal slurry is formed by coal powder with a particle size of less than 74 μm, a hydrogen-donating solvent and a catalyst according to a certain ratio. In other embodiments, the liquid can also be Other liquids that need to measure rheological properties in petroleum, chemical and other fields. The high-temperature and high-pressure system described in this embodiment includes a miniature high-pressure react...

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Abstract

The invention discloses a high-pressure high-temperature liquid viscosity measuring device and method. The measuring device comprises a high-pressure high-temperature system and a measuring system, wherein the measuring system comprises a driving motor, a torque sensor, a driving magnetic barrel, an induced magnetism barrel, a rotating shaft and a stirring paddle; one end of the torque sensor is connected with the driving motor, the other end of the torque sensor is connected with the driving magnetic barrel, and the driving magnetic barrel rotates along the torque sensor; the induced magnetism barrel is positioned in the driving magnetic barrel and can rotate along the driving magnetic barrel under the magnetic action; one end of the rotating shaft is connected with one end, which is far from the torque sensor, of the induced magnetism barrel, the other end of the rotating shaft is connected with the stirring paddle, and a part of the rotating shaft is positioned in the high-pressure high-temperature system; the stirring paddle is positioned in the high-pressure high-temperature system, and the stirring paddle comprises multiple blades which are symmetrically arranged around the rotating shaft. The measuring device provided by the invention can accurately detect the liquid viscosity under a high-pressure high-temperature condition.

Description

technical field [0001] The invention relates to a high-temperature and high-pressure liquid viscosity measuring device and a measuring method, which belong to the field of measuring the fluidity of high-temperature and high-pressure liquids, in particular to a viscosity measuring device and a measuring method suitable for non-Newtonian fluids in an unstable state, especially oil-coal slurry . Background technique [0002] China is a country rich in coal and poor in oil. In recent years, due to the sharp rise in world oil prices and the continuous consumption of domestic oil resources, China needs to import more than half of its oil every year, and its dependence on foreign countries is high. No matter from an economic or strategic point of view See, there is a need to find an alternative that can partially replace petroleum fuels. [0003] Lignite or young bituminous coal can be transformed into liquid fuels and other chemicals by pyrolysis and hydrogenation in a reactor un...

Claims

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Application Information

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IPC IPC(8): G01N11/14
Inventor 颜丙峰吴艳李培霖张晓静毛学锋王雨王勇赵渊钟金龙黄澎石智杰胡发亭张帆孙竟晔李伟林赵鹏
Owner CCTEG CHINA COAL RES INST
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