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Method for extracting soil heavy metal ion

A heavy metal ion and soil technology, which is applied in the pre-treatment field of detection, can solve the problems of cumbersome operation, long time-consuming, complicated operation, etc., and achieve the effect of reducing equipment, improving work efficiency, and simplifying the operation process

Inactive Publication Date: 2014-06-11
CHINA AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Our country has a vast land area, and we want to establish an information record and information traceability system in the process of agricultural product production, processing, storage, sales, and consumption, that is, the process tracking from "farm to table" or the source traceability technology from "table to farmland" , it is necessary to solve the problems of long time-consuming, complicated operation and environmental pollution in the pre-treatment process of the portable heavy metal detection instrument.
[0003] The traditional treatment method has the following problems: (1) The operation is cumbersome, time-consuming, and the extraction process requires high-temperature heating treatment; (2) The ratio of the extraction agent is complex, and the storage requirements are high. Leakage is harmful to the human body and easily causes damage to farmland soil and water The environment is easy to cause secondary pollution; (3) The leaching solution used for detection must undergo secondary pH adjustment before it can be used for equipment detection, and the process operation is complicated

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0022] Below in conjunction with the examples, the specific implementation of the present invention will be further described in detail.

[0023] Divide the plot to be detected into several small dry slices, and the area of ​​each slice is determined according to the actual situation (if the soil is relatively uniform, the area can be increased appropriately; on the contrary, the area is smaller); the arrangement of small-area sampling points is suitable for diagonal , a large area adopts a checkerboard pattern; when sampling soil, first use a small soil shovel to remove about 3 mm of soil on the surface, use a soil sampler to collect soil samples from the plow layer, and cut a soil sample vertically downward at a depth of 20 cm. Take the same amount of soil from the soil samples collected by point blocks and mix them evenly to form a soil sample; evenly disperse the soil samples into ceramic containers, put them in a drying oven at a high temperature of 300 degrees Celsius (th...

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Abstract

The invention relates to a method for extracting a soil heavy metal ion. The method comprises the following steps: preparing an extraction salt solution with the pH value of 4.5, mixing collected soil, carrying out high-temperature forced air drying, grinding dried soil with a soil grinder, weighing part of ground soil, adding a certain amount of an extracting agent, carrying out heating and ultrasound treatment in an ultrasonic instrument, filtering impurities in the soil by adopting a two-step method, carrying out preliminary filtration with a large-aperture filter, then carrying out secondary filtration with a small-aperture rapid filter, removing the tiny impurities in the soil to obtain sample liquid to be tested. By adopting the method, the conventional operation procedure can be simplified, and the extracting efficiency of the heavy metal ion can be improved.

Description

technical field [0001] The invention relates to soil detection technology, in particular to a pretreatment method for detection of soil heavy metal ions. Background technique [0002] Due to the lack of attention paid to environmental protection in the process of industrial and agricultural production development in my country, environmental pollution has become increasingly serious, especially the environment of agricultural product production areas (such as farmland soil and irrigation water), which are closely related to people's lives, suffers the most serious damage from heavy metal pollution. Heavy metal pollutants can cause physiological dysfunction and nutritional imbalance in plants. They have little mobility in the soil and cannot be degraded in nature. After entering the human body through the food chain, they are potentially harmful. Our country has a vast land area, and we want to establish an information record and information traceability system in the process...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28B01D11/02
Inventor 刘刚王辉王志强张志豪
Owner CHINA AGRI UNIV
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