Core-shell type composite fire-extinguishing powder and preparation method thereof
A composite powder, core-shell structure technology, applied in fire protection equipment and other directions, can solve the problems of large particle size, fast particle settling, slow decomposition speed, etc., achieves broad practical application prospects, simple preparation process, and reduces fire extinguishing costs.
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Embodiment 1
[0016] Embodiment 1: after ball milling 140g 13X type zeolite in a ball mill for 30min, its average particle diameter reaches below 10 μm; get this refined zeolite 120g and put it into 20L sodium bicarbonate concentration in the aqueous solution of 0.01mol / L, at a speed Stir mechanically at a speed of 400r / min for 6h, then vacuum freeze-dry the solution at a temperature of -10°C and a pressure of 5.0Pa, then add 1.0g of silicon dioxide and 2.0g of talc, and mix well , to obtain the composite powder fire extinguishing agent of the present invention.
[0017] As measured by a particle size analyzer, the average particle size of the particles in the fire extinguishing agent is 8.6 μm.
[0018] Put 100g of the composite powder in a 1.0L powder storage tank, pressurize it to 0.6MPa, and spray it onto a gasoline fire with an oil pan diameter of 30cm and a flame power of 200kW. The fire extinguishing time is 3.5s, and the amount of fire extinguishing agent is 36.2 g. Under the same...
Embodiment 2
[0019] Example 2: After milling 240g of mordenite in a ball mill for 60min, dry it at 120°C for 2h; take 200g of the refined zeolite and put it into 20L of potassium bicarbonate solution with a concentration of 0.025mol / L at a speed of 500r / L Stir mechanically at a speed of min for 8 hours, then vacuum freeze-dry the solution at a temperature of -15°C and a pressure of 10.0Pa, then add 2.5g of silicon dioxide and 4.5g of talcum powder, and mix evenly to obtain The composite powder fire extinguishing agent of the present invention.
[0020] As measured by a particle size analyzer, the average particle size of the particles in the fire extinguishing agent is 7.5 μm.
[0021] 100g of the composite powder is packed in a 1.0L powder storage tank, pressurized to 0.6MPa, sprayed onto a fire source with an oil pan diameter of 40cm, a thickness of edible oil of 5cm, and a flame power of 70kW. The average fire extinguishing time is 5.0 s, the average amount of fire extinguishing agent ...
Embodiment 3
[0022] Example 3: After ball milling 350g of 4A type zeolite in a ball mill for 90min, dry at 120°C for 2h; take 300g of the refined zeolite and put it into 30L of ammonium dihydrogen phosphate concentration in an aqueous solution of 0.015mol / L, at a speed of Stir mechanically at a speed of 600r / min for 12h, then vacuum freeze-dry the solution at a temperature of -20°C and a pressure of 8.0Pa, then add 4.0g of silicon dioxide and 8.0g of talc, mix well, That is the composite powder fire extinguishing agent of the present invention.
[0023] As measured by a particle size analyzer, the average particle size of the particles in the fire extinguishing agent is 8.2 μm.
[0024] Put 100g of the composite powder in a 1.0L powder storage tank, pressurize it to 0.6MPa, and spray it onto a gasoline fire with an oil pan diameter of 30cm and a flame power of 200kW. The fire extinguishing time is 3.0s, and the amount of fire extinguishing agent is 31.2 g. Under the same experimental con...
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