Method for preparing essence sustained-release porous capsule from bentonite
A technology of porous capsule and bentonite, applied in the fields of hygiene and materials, to achieve the effect of strong operability, easy access, and strong market competitiveness
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[0020] The specific steps of the preparation method for preparing essential oil sustained-release porous capsules by using bentonite are as follows:
[0021] (1) Add bentonite to a certain amount of deionized water according to the formula, stir and heat to 60°C, and stir for 30 minutes;
[0022] (2) Add a certain amount of surfactant (sodium α-olefin sulfonate and cetyl dimethyl benzyl ammonium chloride in a certain proportion) according to the formula, and stir for 3 hours at a constant temperature of 60°C;
[0023] (3) Take it out after natural cooling, carry out centrifugation, and wash with 50% alcohol solution;
[0024] (4) Dry in an oven at 100°C, and pass through a 200-mesh sieve after grinding to obtain organic bentonite;
[0025] (5) Then add the organic bentonite to the sodium alginate solution with a concentration of 2% according to the mass ratio, and after stirring for 30 minutes, add the obtained solution dropwise to the calcium chloride solution with a concent...
Embodiment 1
[0028] The weight ratio of the raw material formula: bentonite is 77 wt%, aroma improver is 23wt%, weigh the two raw materials according to the formula, first add bentonite to a certain amount of deionized water and heat to 60°C, stir for 30 minutes; add a certain amount of A certain amount of surfactant (sodium α-olefin sulfonate and hexadecyl dimethyl benzyl ammonium chloride in a ratio of 3:7), stirred at 60°C for 3 hours; after natural cooling, take it out and carry out centrifugation , washed with 50% alcohol aqueous solution; dried in an oven at 100°C, ground and passed through a 200-mesh sieve to obtain organic bentonite, then added organic bentonite to 2% sodium alginate solution according to the mass ratio, and stirred for 30 minutes , the resulting solution was added dropwise to a calcium chloride solution with a concentration of 7%, and the obtained granules were washed and dried in an oven at 35°C to obtain the essential oil sustained-release porous capsule, namely ...
Embodiment 2
[0030] The weight ratio of the raw material formula: bentonite is 69 wt%, aroma improver is 31wt%, weigh the two raw materials according to the formula, first add bentonite to a certain amount of deionized water and heat to 65°C, stir for 30 minutes; add a certain amount of amount of surfactant (sodium α-olefin sulfonate and hexadecyl dimethyl benzyl ammonium chloride in a ratio of 4:6), stirred at 65°C for 4 hours; after natural cooling, take it out and perform centrifugation , washed with 50% alcohol aqueous solution; dried in an oven at 100°C, ground and passed through a 200-mesh sieve to obtain organic bentonite, then added organic bentonite to 2% sodium alginate solution according to the mass ratio, and stirred for 30 minutes , the resulting solution was added dropwise to a calcium chloride solution with a concentration of 7%, and the obtained granules were washed and dried in an oven at 35°C to obtain the essential oil sustained-release porous capsule, namely the essentia...
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